ethyl ester of 3-butoxy-2-propen-1-oic acid

Base Information

• Chemical Name: ethyl ester of 3-butoxy-2-propen-1-oic acid
• CAS No.: 74649-08-4
• Molecular Formula: C₉H₁₆O₃
• Molecular Weight: 172.224
• Mol file: 74649-08-4.mol

Synonyms:

Chemical Property of ethyl ester of 3-butoxy-2-propen-1-oic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ethyl ester of 3-butoxy-2-propen-1-oic acid

There total 1 articles about ethyl ester of 3-butoxy-2-propen-1-oic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 3-ethoxyacrylate (1001-26-9) → ethyl ester of 3-butoxy-2-propen-1-oic acid (74649-08-4) + β-n-Butoxyacrylsaeure-n-butylester (16722-19-3)

Guidance literature:

analoge Reaktionen mit weiteren Alkoholen;

DOI:10.1021/ja01176a041

Reference yield:

ethyl ester of 3-butoxy-2-propen-1-oic acid (74649-08-4) → β-Butoxy-propionsaeure-ethylester (14144-46-8)

Guidance literature:

With alcoholmoist Raney nickel; at 50 ℃; under 73550.8 Torr; Hydrogenation;

DOI:10.1021/ja01176a041

Reference yield:

ethyl ester of 3-butoxy-2-propen-1-oic acid (74649-08-4) → 3-Butyloxypropanoic acid (7420-06-6)

Guidance literature:

Multi-step reaction with 2 steps

1: alcoholmoist Raney nickel / 50 °C / 73550.8 Torr / Hydrogenation

2: diluted NaOH

With sodium hydroxide; alcoholmoist Raney nickel;

DOI:10.1021/ja01176a041

upstream raw materials:

ethyl 3-ethoxyacrylate

Downstream raw materials:

β-Butoxy-propionsaeure-ethylester

3-Butyloxypropanoic acid