triphenylstannyl triphenylstannanedithiocarboxylate

Base Information

Chemical Name:triphenylstannyl triphenylstannanedithiocarboxylate
CAS No.:107557-47-1
Molecular Formula:C₃₇H₃₀S₂Sn₂
Molecular Weight:776.197
Hs Code.:

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Suppliers and Price of triphenylstannyl triphenylstannanedithiocarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of triphenylstannyl triphenylstannanedithiocarboxylate

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Technology Process of triphenylstannyl triphenylstannanedithiocarboxylate

There total 1 articles about triphenylstannyl triphenylstannanedithiocarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 639-58-7
triphenyltin chloride

: 107557-47-1
triphenylstannyl triphenylstannanedithiocarboxylate

Guidance literature:: With carbon disulfide; lithium; In tetrahydrofuran; 1,4-dioxane; reaction of Ph3SnCl with Li in THF, sepg. of the excess of Li, addn. of CS2 in dioxane over 30 min, chromy. on silicagel (THF/ether), addn. of Ph3SnCl, stirring for 5 h, all steps under Ar; evapn. of the solvent, chromy. on silicagel (ether), recrystn. (toluene), elem. anal.;

Reference yield: 61.0%

: 14040-11-0
tungsten hexacarbonyl

: 107557-47-1
triphenylstannyl triphenylstannanedithiocarboxylate

: 107557-54-0
pentacarbonyl(triphenylstannyl triphenylstannanedithiocarboxylate)tungsten

Guidance literature:: With C₄H₈O; In tetrahydrofuran; reaction of the ester with the activated metalcarbonyle in THF under Ar; evapn. of the solvent, chromy. on silicagel (THF/petroleum ether), recrystn. (n-hexane), elem. anal.;