Cu(B₄H₉){P(C₆H₅)3}2

Base Information

Chemical Name:Cu(B₄H₉){P(C₆H₅)3}2
CAS No.:69680-95-1
Molecular Formula:C₃₆H₃₉B₄CuP₂
Molecular Weight:640.443
Hs Code.:

Cu(B<sub>4</sub>H<sub>9</sub>){P(C<sub>6</sub>H<sub>5</sub>)3}2

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Chemical Property of Cu(B₄H₉){P(C₆H₅)3}2

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Technology Process of Cu(B₄H₉){P(C₆H₅)3}2

There total 3 articles about Cu(B₄H₉){P(C₆H₅)3}2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 15709-76-9
tris(triphenylphosphino)copper(I) chloride

: K⁽¹⁺⁾*B₅H₁₂^(1-)=K{B₅H₁₂}

: 69680-95-1
Cu(B₄H₉){P(C₆H₅)3}2

Guidance literature:: byproducts: BH3*P(C6H5)3;

Reference yield: 51.0%

: tetraborane

: 36273-10-6
Cu⁽¹⁺⁾*Br^(1-)*2P(C₆H₅)3*0.5C₆H₆={CuBr{P(C₆H₅)3}2*0.5C₆H₆}

: 69680-95-1
Cu(B₄H₉){P(C₆H₅)3}2

Guidance literature:: With KH; In tetrahydrofuran; dichloromethane; byproducts: H2, KBr, C6H6; B4H10 and Me2O condensed in a react. vessel contg. KH at -196°C, stirred at -78°C, 30 min; evapn o Me2O; addn. of THF and CH2Cl2, -196°C; addn. of the Cu complex at -78°C; stirred at -45°C to -78°C for ca 19 h;; Et2O condensed onto the mixt. at -78°C and filtered at -78°C; ppt. washed (cold Et2O), dissoled in CH2Cl2; KBr filtered off; concd. at -23°C; pptn. by addn. of Et2O at -78°C; washed (Et2O, pentane); elem. anal.;;

Reference yield: 30.0%

: tetraborane

: 15709-76-9
tris(triphenylphosphino)copper(I) chloride

: 69680-95-1
Cu(B₄H₉){P(C₆H₅)3}2

Guidance literature:: With KH; In tetrahydrofuran; dichloromethane; byproducts: H2, KCl, P(C6H5)3; B4H10 and Me2O condensed in a react. vessel charged with KH at -196°C; stirred at -78°C for 15 min, evapn. of Me2O at -78°C; addn. of THF, Cu complex and CH2Cl2 at -196°C; stirred at -45°C to -78°C for 19 h;; Et2O condensed onto the mixt. at -78°C; filtered at -78°C, ppt. washed (cold Et2O), dissolved in CH2Cl2; KCl filtered off; concn. at -23°C and pptn. by addn. of Et2O at -78°C; washed (Et2O, pentane); elem. anal.;;