(N,N'-bis(2,3,5,6-tetrafluorophenyl)ethane-1,2-diaminato^(2-))dipyridineplatinum(II)*Me₂CO

Base Information

• Chemical Name: (N,N'-bis(2,3,5,6-tetrafluorophenyl)ethane-1,2-diaminato^(2-))dipyridineplatinum(II)*Me₂CO
• CAS No.: 92181-59-4
• Molecular Formula: C₃H₆O*C₂₄H₁₆F₈N₄Pt
• Molecular Weight: 765.565

Synonyms:

Chemical Property of (N,N'-bis(2,3,5,6-tetrafluorophenyl)ethane-1,2-diaminato^(2-))dipyridineplatinum(II)*Me₂CO

Chemical Property:

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Technology Process of (N,N'-bis(2,3,5,6-tetrafluorophenyl)ethane-1,2-diaminato^(2-))dipyridineplatinum(II)*Me₂CO

There total 4 articles about (N,N'-bis(2,3,5,6-tetrafluorophenyl)ethane-1,2-diaminato^(2-))dipyridineplatinum(II)*Me₂CO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

dichloro(ethylenediamine)platinum(II) (14096-51-6) + thallous 2,3,5,6-tetrafluorobenzoate (75669-81-7) + Pentafluorobenzene (363-72-4) → [N,N'-bis(2,3,5,6-tetrafluorophenyl)ethane-1,2-diaminato]dipyridineplatinum(II)-acetone (1/1) (92181-59-4)

Guidance literature:

With acetone; In pyridine; byproducts: TlCl, CO2; TlO2C(p-HC6F4) and Pt(en)Cl2 and HC6F5 were stirred together in pyridine under N2 at 115°C for 15 min; pyridine was evapd., residue was stirred with light petroleum to removetraces of pyridine, then was extd. with ether, extract was filtered, residue was evapd. and crystd.; elem. anal.;

Reference yield: 37.0%

dichloro(ethylenediamine)platinum(II) (14096-51-6) + thallium(I) pentafluorobenzoate (68558-86-1) → [N,N'-bis(2,3,5,6-tetrafluorophenyl)ethane-1,2-diaminato]dipyridineplatinum(II)-acetone (1/1) (92181-59-4)

Guidance literature:

With acetone; In pyridine; byproducts: TlCl, CO2; TlO2CC6F5 and Pt(en)Cl2 were stirred together in pyridine under N2 at 115°C for 60 min; pyridine was evapd., residue was stirred with light petroleum to removetraces of pyridine, then was extd. with ether, extract was filtered, residue was evapd. and crystd.; elem. anal.;

Reference yield: 37.0%

dichloro(ethylenediamine)-platinum(II) (14096-51-6) + thallium(I) pentafluorobenzoate (68558-86-1) → (C6F5)PtCl(NH2CH2CH2NH2) + (N,N'-bis(2,3,5,6-tetrafluorophenyl)ethane-1,2-diaminato(2-))dipyridineplatinum(II)*Me2CO (92181-59-4) + (C6F5)2Pt(NH2CH2CH2NH2) (112084-19-2)

Guidance literature:

With pyridine; acetone; In pyridine; acetone; byproducts: CO2; react. stoich. amt. PtCl2en with TlO2CC6F5 in boiling pyridine for 60 min under N2, mixt. evapd. to dryness, extd. with acetone, filtered; crystn. from acetone-petroleum ether;

DOI:10.1016/S0277-5387(00)88017-1

upstream raw materials:

dichloro(ethylenediamine)platinum(II)

thallous 2,3,5,6-tetrafluorobenzoate

Pentafluorobenzene

thallium(I) pentafluorobenzoate

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