1-hexahydro-2-(4-methoxybenzoyl)pyridazin

Base Information

Chemical Name:1-hexahydro-2-(4-methoxybenzoyl)pyridazin
CAS No.:112549-67-4
Molecular Formula:C₂₀H₁₉N₅O₅
Molecular Weight:409.401
Hs Code.:

1-<Diazo(4-nitrophenyl)acetyl>hexahydro-2-(4-methoxybenzoyl)pyridazin

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-hexahydro-2-(4-methoxybenzoyl)pyridazin

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Technology Process of 1-hexahydro-2-(4-methoxybenzoyl)pyridazin

There total 3 articles about 1-hexahydro-2-(4-methoxybenzoyl)pyridazin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 112549-62-9
Hexahydro-1-(4-methoxybenzoyl)-2-(4-nitrophenylacetyl)pyridazin

: 112549-67-4
1-hexahydro-2-(4-methoxybenzoyl)pyridazin

Guidance literature:: With 4-toluenesulfonyl azide; triethylamine; In acetonitrile; for 16h; Ambient temperature;

Reference yield:

: 100-09-4
4-methoxybenzoic acid

: 112549-67-4
1-hexahydro-2-(4-methoxybenzoyl)pyridazin

Guidance literature:: Multi-step reaction with 3 steps

1: 37 percent / dicyclohexylcarbodiimide, 4-(dimethylamino)pyridine / benzene / 16 h / 40 °C

2: toluene / 12 h / Heating

3: 72 percent / Et₃N, tosylazide / acetonitrile / 16 h / Ambient temperature

With dmap; 4-toluenesulfonyl azide; triethylamine; dicyclohexyl-carbodiimide; In toluene; acetonitrile; benzene;

Reference yield:

: 112575-00-5
Hexahydro-1-(4-methoxybenzoyl)pyridazin

: 112549-67-4
1-hexahydro-2-(4-methoxybenzoyl)pyridazin

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 12 h / Heating

2: 72 percent / Et₃N, tosylazide / acetonitrile / 16 h / Ambient temperature

With 4-toluenesulfonyl azide; triethylamine; In toluene; acetonitrile;