5-(4-methoxy-phenylethylene)-2-nitrobenzyl alcohol

Base Information

Chemical Name:5-(4-methoxy-phenylethylene)-2-nitrobenzyl alcohol
CAS No.:914777-96-1
Molecular Formula:C₁₆H₁₅NO₄
Molecular Weight:285.299
Hs Code.:

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Chemical Property of 5-(4-methoxy-phenylethylene)-2-nitrobenzyl alcohol

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Technology Process of 5-(4-methoxy-phenylethylene)-2-nitrobenzyl alcohol

There total 3 articles about 5-(4-methoxy-phenylethylene)-2-nitrobenzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 637-69-4,24936-44-5
4-Methoxystyrene

: 150022-33-6
(5-iodo-2-nitrophenyl)methanol

: 914777-96-1
5-(4-methoxy-phenylethylene)-2-nitrobenzyl alcohol

Guidance literature:: With silver nitrate; triethylamine; triphenylphosphine; palladium diacetate; In acetonitrile; for 120h; Heating;
DOI:10.1002/chem.200501393

Reference yield:

: 13280-60-9
5-amino-2-nitrobenzoic acid

: 914777-96-1
5-(4-methoxy-phenylethylene)-2-nitrobenzyl alcohol

Guidance literature:: Multi-step reaction with 3 steps

1.1: tert-butyl nitrite; boron trifluoride etherate / tetrahydrofuran / -15 - 5 °C

1.2: sodium iodide / acetone / 12 h / 20 °C

2.1: 90 percent / borane / tetrahydrofuran / 1 h / Heating

3.1: 34 percent / silver nitrate; triphenylphosphine; triethylamine / palladium acetate / acetonitrile / 120 h / Heating

With tert.-butylnitrite; boron trifluoride diethyl etherate; borane; silver nitrate; triethylamine; triphenylphosphine; palladium diacetate; In tetrahydrofuran; acetonitrile;
DOI:10.1002/chem.200501393

Reference yield:

: 35674-28-3
5-iodo-2-nitrobenzoic acid

: 914777-96-1
5-(4-methoxy-phenylethylene)-2-nitrobenzyl alcohol

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / borane / tetrahydrofuran / 1 h / Heating

2: 34 percent / silver nitrate; triphenylphosphine; triethylamine / palladium acetate / acetonitrile / 120 h / Heating

With borane; silver nitrate; triethylamine; triphenylphosphine; palladium diacetate; In tetrahydrofuran; acetonitrile;
DOI:10.1002/chem.200501393