2-(12-benzyloxy-1-methoxydodecyl)cyclohexanone

Base Information

• Chemical Name: 2-(12-benzyloxy-1-methoxydodecyl)cyclohexanone
• CAS No.: 1359738-14-9
• Molecular Formula: C₂₆H₄₂O₃
• Molecular Weight: 402.618

Synonyms:

Chemical Property of 2-(12-benzyloxy-1-methoxydodecyl)cyclohexanone

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 2-(12-benzyloxy-1-methoxydodecyl)cyclohexanone

There total 4 articles about 2-(12-benzyloxy-1-methoxydodecyl)cyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

12-hydroxy-1-dodecanal dimethylacetal (873958-87-3) → 2-(12-benzyloxy-1-methoxydodecyl)cyclohexanone (1359738-14-9)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydride / tetrahydrofuran / 22 h / 20 °C / Inert atmosphere

2: dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3: dichloromethane / 2 h / 20 °C / Inert atmosphere

With sodium hydride; In tetrahydrofuran; dichloromethane;

DOI:10.1002/asia.201100812

Reference yield:

benzyl bromide (100-39-0) → 2-(12-benzyloxy-1-methoxydodecyl)cyclohexanone (1359738-14-9)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydride / tetrahydrofuran / 22 h / 20 °C / Inert atmosphere

2: dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3: dichloromethane / 2 h / 20 °C / Inert atmosphere

With sodium hydride; In tetrahydrofuran; dichloromethane;

DOI:10.1002/asia.201100812

Reference yield:

1-(1-Cyclohexen-1-yl)pyrrolidine (1125-99-1) + CF3O3S(1-)*C28H44NO2(1+) → 2-(12-benzyloxy-1-methoxydodecyl)cyclohexanone (1359738-14-9)

Guidance literature:

In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1002/asia.201100812

upstream raw materials:

12-hydroxy-1-dodecanal dimethylacetal

1-(1-Cyclohexen-1-yl)pyrrolidine

((12,12-dimethoxydodecyloxy)methyl)benzene

benzyl bromide

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