[Pd2(OAc)2(μ-C,N,N'-C(=NXy)C6H4NH2-2)]2

Base Information

Chemical Name:[Pd2(OAc)2(μ-C,N,N'-C(=NXy)C6H4NH2-2)]2
CAS No.:1351465-86-5
Molecular Formula:C₃₄H₃₆N₄O₄Pd₂
Molecular Weight:777.524
Hs Code.:

Synonyms:

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Chemical Property of [Pd2(OAc)2(μ-C,N,N'-C(=NXy)C6H4NH2-2)]2

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Technology Process of [Pd2(OAc)2(μ-C,N,N'-C(=NXy)C6H4NH2-2)]2

There total 3 articles about [Pd2(OAc)2(μ-C,N,N'-C(=NXy)C6H4NH2-2)]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: [PdCl₂(C,N-C(=NHXy)C₆H₄NH₂-2)]

: 127-09-3
sodium acetate

: 1351465-86-5
[Pd2(OAc)2(μ-C,N,N'-C(=NXy)C6H4NH2-2)]2

Guidance literature:: With TlOSO₂CF₃; In acetone; TlOSO2CF3 was added to a suspn. of complex in acetone, stirred for 1.5 h, filtered, NaOCOCH3 was added, stirred for 4 h; filtered, concd. under vac., diethyl ether was added, filtered, washed with diethyl ether (3x), dried by suction and then in an over under vac. (70°C, 6 h); elem. anal.;
DOI:10.1021/om200986k

Reference yield:

: 1035630-25-1
[Pd(C,N,O-C(=N(C₆H₃Me₂-2,6))C₆H₄(NC(Me)CHC(Me)O)-2)(PPh₃)]

: 1351465-86-5
[Pd2(OAc)2(μ-C,N,N'-C(=NXy)C6H4NH2-2)]2

Guidance literature:: Multi-step reaction with 2 steps

1: H₂O₂ / dichloromethane; water

2: TlOSO₂CF₃ / acetone

With H₂O₂; TlOSO₂CF₃; In dichloromethane; water; acetone;
DOI:10.1021/om200986k

Reference yield:

: [PdCl₂(=NHXy)C₆H₄NH₃-2)(PPh₃)]Cl

: 1351465-86-5
[Pd2(OAc)2(μ-C,N,N'-C(=NXy)C6H4NH2-2)]2

Guidance literature:: Multi-step reaction with 3 steps

1: triethyl amine

2: C(CH₃)3OOH

3: TlOSO₂CF₃ / acetone

With triethyl amine; C(CH₃)3OOH; TlOSO₂CF₃; In acetone;
DOI:10.1021/om200986k