2--4,5-dihydro-4,4-diphenyl-5-(isopropylimino)thiazole

Base Information

Chemical Name:2--4,5-dihydro-4,4-diphenyl-5-(isopropylimino)thiazole
CAS No.:124512-22-7
Molecular Formula:C₂₈H₃₀N₄O₂S
Molecular Weight:486.638
Hs Code.:

2-<tert-butyl(2-nitrophenyl)amino>-4,5-dihydro-4,4-diphenyl-5-(isopropylimino)thiazole

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Chemical Property of 2--4,5-dihydro-4,4-diphenyl-5-(isopropylimino)thiazole

Chemical Property:

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Technology Process of 2--4,5-dihydro-4,4-diphenyl-5-(isopropylimino)thiazole

There total 5 articles about 2--4,5-dihydro-4,4-diphenyl-5-(isopropylimino)thiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 598-45-8
i-propyl isocyanide

: 124512-07-8
2--4,4-diphenyl-1-thia-3-azabuta-1,3-diene

: 124512-22-7
2--4,5-dihydro-4,4-diphenyl-5-(isopropylimino)thiazole

Guidance literature:: In acetonitrile; for 4h; Heating;
DOI:10.1021/jo00293a011

Reference yield:

: 1013-88-3
Benzophenone imine

: 124512-22-7
2--4,5-dihydro-4,4-diphenyl-5-(isopropylimino)thiazole

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / NEt₃ / tetrahydrofuran / 6 h / Ambient temperature

2: 68 percent / toluene / 72 h / Heating

3: 77 percent / acetonitrile / 4 h / Heating

With triethylamine; In tetrahydrofuran; toluene; acetonitrile;
DOI:10.1021/jo00293a011

Reference yield:

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 124512-22-7
2--4,5-dihydro-4,4-diphenyl-5-(isopropylimino)thiazole

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran

2: 90 percent / NEt₃ / tetrahydrofuran / 6 h / Ambient temperature

3: 68 percent / toluene / 72 h / Heating

4: 77 percent / acetonitrile / 4 h / Heating

With triethylamine; In tetrahydrofuran; toluene; acetonitrile;
DOI:10.1021/jo00293a011