(Pd(C₆H₅CONHNCHC₆H₂(OCH₃)2)Cl)

Base Information

Chemical Name:(Pd(C₆H₅CONHNCHC₆H₂(OCH₃)2)Cl)
CAS No.:676325-88-5
Molecular Formula:C₁₆H₁₅ClN₂O₃Pd
Molecular Weight:425.18
Hs Code.:

(Pd(C<sub>6</sub>H<sub>5</sub>CONHNCHC<sub>6</sub>H<sub>2</sub>(OCH<sub>3</sub>)2)Cl)

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Chemical Property of (Pd(C₆H₅CONHNCHC₆H₂(OCH₃)2)Cl)

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Technology Process of (Pd(C₆H₅CONHNCHC₆H₂(OCH₃)2)Cl)

There total 1 articles about (Pd(C₆H₅CONHNCHC₆H₂(OCH₃)2)Cl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: palladium dichloride

: 329069-36-5
N-(benzoyl)-N'-(2,4-dimethoxybenzylidene)hydrazine

: 676325-88-5
(Pd(C₆H₅CONHNCHC₆H₂(OCH₃)2)Cl)

Guidance literature:: With LiCl; In methanol; mixt. PdCl2 and LiCl in MeOH was refluxed for 1 h, cooled to room temp. and filtered, filtrate was added dropwise to soln. N-(benzoyl)-N'-(2,4-dimethoxybenzylidene)hydrazine in MeOH and stirred at room temp. for 3 days and refluxed for 3 days; ppt. was filtered, washed with MeOH and dried in air; elem. anal.;
DOI:10.1016/j.jorganchem.2003.10.022

Reference yield: 80.0%

: 676325-88-5
(Pd(C₆H₅CONHNCHC₆H₂(OCH₃)2)Cl)

: 603-35-0
triphenylphosphine

: 676325-90-9
(Pd(C₆H₅CONNCHC₆H₂(OCH₃)2)(P(C₆H₅)3))

Guidance literature:: In methanol; acetonitrile; Pd complex in MeOH-MeCN mixt. was stirred at room temp. for 3 h, PPh3 was added and stirred at room temp. for 2 days; ppt. was filtered, washed with MeOH and dried in air; elem. anal.;
DOI:10.1016/j.jorganchem.2003.10.022

Reference yield: 48.0%

: 676325-88-5
(Pd(C₆H₅CONHNCHC₆H₂(OCH₃)2)Cl)

: 603-35-0
triphenylphosphine

: 676325-91-0
(PdCl(C₆H₅CONHNCHC₆H₂(OCH₃)2)(P(C₆H₅)3))

Guidance literature:: In methanol; acetonitrile; to suspn. Pd complex in MeOH-MeCN mixt. PPh3 was added and stirred at room temp. for 10 h; ppt. was filtered, washed with MeOH and dried in air; elem. anal.;
DOI:10.1016/j.jorganchem.2003.10.022