C₂₀H₂₃N₃O₄S

Base Information

Chemical Name:C₂₀H₂₃N₃O₄S
CAS No.:1426329-59-0
Molecular Formula:C₂₀H₂₃N₃O₄S
Molecular Weight:401.486
Hs Code.:

C<sub>20</sub>H<sub>23</sub>N<sub>3</sub>O<sub>4</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₀H₂₃N₃O₄S

Chemical Property:

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Technology Process of C₂₀H₂₃N₃O₄S

There total 7 articles about C₂₀H₂₃N₃O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90-76-6,90-77-7,530-23-4,579-32-8,579-33-9,643-68-5,2596-19-2,6490-68-2,6490-70-6,6490-72-8,6490-73-9,6490-74-0,14196-84-0,14196-86-2,14257-69-3,58381-21-8
2-deoxy-2-amino glucose

: 1426329-59-0
C₂₀H₂₃N₃O₄S

Guidance literature:: Multi-step reaction with 7 steps

1: triflic azide; potassium carbonate; copper(II) sulfate / water; methanol / 24 h

2: triethylamine; dmap / dichloromethane / 2 h / 20 °C

3: boron trifluoride diethyl etherate / chloroform / 0 - 40 °C

4: sodium methylate; water / methanol / 1.5 h

5: toluene-4-sulfonic acid / acetonitrile / 2 h

6: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C / Inert atmosphere

7: methanol; camphor-10-sulfonic acid / 2 h / 20 °C

With methanol; dmap; triflic azide; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; water; sodium methylate; sodium hydride; potassium carbonate; toluene-4-sulfonic acid; copper(II) sulfate; triethylamine; In methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1039/c3ob26994a

Reference yield:

: C₂₇H₂₇N₃O₄S

: 1426329-59-0
C₂₀H₂₃N₃O₄S

Guidance literature:: With methanol; camphor-10-sulfonic acid; at 20 ℃; for 2h; stereoselective reaction;
DOI:10.1039/c3ob26994a

Reference yield:

: 171032-74-9
1,3,4,6-tetra-O-acetyl-2-azido-2-deoxy-D-glucopyranose

: 1426329-59-0
C₂₀H₂₃N₃O₄S

Guidance literature:: Multi-step reaction with 5 steps

1: boron trifluoride diethyl etherate / chloroform / 0 - 40 °C

2: sodium methylate; water / methanol / 1.5 h

3: toluene-4-sulfonic acid / acetonitrile / 2 h

4: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C / Inert atmosphere

5: methanol; camphor-10-sulfonic acid / 2 h / 20 °C

With methanol; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; water; sodium methylate; sodium hydride; toluene-4-sulfonic acid; In methanol; chloroform; N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1039/c3ob26994a