C₂₉H₃₄FN₄O₇S^(1-)*Na⁽¹⁺⁾

Base Information

Chemical Name:C₂₉H₃₄FN₄O₇S^(1-)*Na⁽¹⁺⁾
CAS No.:1309777-96-5
Molecular Formula:C₂₉H₃₄FN₄O₇S*Na
Molecular Weight:624.666
Hs Code.:

C<sub>29</sub>H<sub>34</sub>FN<sub>4</sub>O<sub>7</sub>S<sup>(1-)</sup>*Na<sup>(1+)</sup>

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Chemical Property of C₂₉H₃₄FN₄O₇S^(1-)*Na⁽¹⁺⁾

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Technology Process of C₂₉H₃₄FN₄O₇S^(1-)*Na⁽¹⁺⁾

There total 6 articles about C₂₉H₃₄FN₄O₇S^(1-)*Na⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1319751-86-4
C₃₃H₄₃FN₄O₇S

: 1309777-96-5
C₂₉H₃₄FN₄O₇S^(1-)*Na⁽¹⁺⁾

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; water; at 50 ℃; for 2h;
DOI:10.1016/j.bmcl.2010.11.103

Reference yield:

: 1319747-57-3
C₂₆H₂₃NO₃

: 1309777-96-5
C₂₉H₃₄FN₄O₇S^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 6 steps

1: triethylamine / dichloromethane / 0.5 h / 0 °C

2: toluene-4-sulfonic acid; acetic acid / 5,5-dimethyl-1,3-cyclohexadiene / 16 h / Reflux

3: palladium 10% on activated carbon; hydrogen / methanol / 4 h / 25 °C

4: 1,1'-carbonyldiimidazole / N,N-dimethyl-formamide / 2 h / 0 - 20 °C

5: Acidic conditions

6: sodium hydroxide / tetrahydrofuran; water / 2 h / 50 °C

With palladium 10% on activated carbon; hydrogen; toluene-4-sulfonic acid; acetic acid; triethylamine; 1,1'-carbonyldiimidazole; sodium hydroxide; In tetrahydrofuran; methanol; 5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2010.11.103

Reference yield:

: 867308-95-0
3-Cyclopropyl-2-(4-fluoro-benzoylamino)-3-oxo-propionic acid benzyl ester

: 1309777-96-5
C₂₉H₃₄FN₄O₇S^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 5 steps

1: toluene-4-sulfonic acid; acetic acid / 5,5-dimethyl-1,3-cyclohexadiene / 16 h / Reflux

2: palladium 10% on activated carbon; hydrogen / methanol / 4 h / 25 °C

3: 1,1'-carbonyldiimidazole / N,N-dimethyl-formamide / 2 h / 0 - 20 °C

4: Acidic conditions

5: sodium hydroxide / tetrahydrofuran; water / 2 h / 50 °C

With palladium 10% on activated carbon; hydrogen; toluene-4-sulfonic acid; acetic acid; 1,1'-carbonyldiimidazole; sodium hydroxide; In tetrahydrofuran; methanol; 5,5-dimethyl-1,3-cyclohexadiene; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2010.11.103