C₂₉H₂₈ClNO₆

Base Information

Chemical Name:C₂₉H₂₈ClNO₆
CAS No.:1314420-19-3
Molecular Formula:C₂₉H₂₈ClNO₆
Molecular Weight:521.997
Hs Code.:

C<sub>29</sub>H<sub>28</sub>ClNO<sub>6</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₂₈ClNO₆

Chemical Property:

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Technology Process of C₂₉H₂₈ClNO₆

There total 7 articles about C₂₉H₂₈ClNO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1314420-17-1
C₃₅H₂₈ClNO₆

: 124-41-4
sodium methylate

: 1314420-19-3
C₂₉H₂₈ClNO₆

Guidance literature:: In tetrahydrofuran; methanol; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/anie.201101621

Reference yield:

: 885592-69-8
(2S,4R,5R)-4-(benzyloxy)-5-((benzyloxy)methyl)-2-methoxydihydrofuran-3(2H)-one

: 1314420-19-3
C₂₉H₂₈ClNO₆

Guidance literature:: Multi-step reaction with 6 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: 0.17 h / -78 °C / Inert atmosphere

2.1: dmap; triethylamine / dichloromethane / 24 h / 20 °C / Inert atmosphere

3.1: boron trifluoride diethyl etherate / nitromethane / 0 - 20 °C / Inert atmosphere

4.1: selenium(IV) oxide / 1,4-dioxane / 36 h / 135 °C / Inert atmosphere

5.1: dihydrogen peroxide; potassium carbonate / tetrahydrofuran / 4 h / 20 °C

6.1: tetrahydrofuran; methanol / 0 - 20 °C / Inert atmosphere

With dmap; selenium(IV) oxide; boron trifluoride diethyl etherate; dihydrogen peroxide; potassium carbonate; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; 1,4-dioxane; methanol; nitromethane; dichloromethane; 1.1: Aldol reaction / 1.2: Aldol reaction;
DOI:10.1002/anie.201101621

Reference yield:

: 1314420-11-5
C₃₇H₃₄ClNO₇

: 1314420-19-3
C₂₉H₂₈ClNO₆

Guidance literature:: Multi-step reaction with 4 steps

1: boron trifluoride diethyl etherate / nitromethane / 0 - 20 °C / Inert atmosphere

2: selenium(IV) oxide / 1,4-dioxane / 36 h / 135 °C / Inert atmosphere

3: dihydrogen peroxide; potassium carbonate / tetrahydrofuran / 4 h / 20 °C

4: tetrahydrofuran; methanol / 0 - 20 °C / Inert atmosphere

With selenium(IV) oxide; boron trifluoride diethyl etherate; dihydrogen peroxide; potassium carbonate; In tetrahydrofuran; 1,4-dioxane; methanol; nitromethane;
DOI:10.1002/anie.201101621