C₃₃H₄₆O₄

Base Information

• Chemical Name: C₃₃H₄₆O₄
• CAS No.: 1373922-46-3
• Molecular Formula: C₃₃H₄₆O₄
• Molecular Weight: 506.726
• Mol file: 1373922-46-3.mol

Synonyms:

Chemical Property of C₃₃H₄₆O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₃H₄₆O₄

There total 1 articles about C₃₃H₄₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

C36H54O4S2 → C33H46O4 + C33H46O4 (1373922-52-1) + C33H46O4 (1373922-46-3)

Guidance literature:

With mercury(II) perchlorate hexahydrate; In dichloromethane; water; acetonitrile; at 0 ℃; for 2h;

DOI:10.1271/bbb.110130

Reference yield:

C19H22O5 (1160697-54-0) + C33H46O4 (1373922-46-3) → C52H66O8

Guidance literature:

C₁₉H₂₂O₅; With 2,4,6-trichlorobenzoyl chloride; triethylamine; In toluene; at 20 ℃; for 2h;

C₃₃H₄₆O₄; With dmap; In toluene; at 50 ℃; for 2h;

DOI:10.1271/bbb.110130

Reference yield:

C33H46O4 (1373922-46-3) → C44H58O7

Guidance literature:

Multi-step reaction with 2 steps

1.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 2 h / 20 °C

1.2: 2 h / 50 °C

2.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 1 h / 20 °C

With 2,4,6-trichlorobenzoyl chloride; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water; toluene;

DOI:10.1271/bbb.110130

Downstream raw materials:

12,12-dimethyl-aplog-1