5-Nitropyrogallol-1,3-dibenzolsulfonat

Base Information

• Chemical Name: 5-Nitropyrogallol-1,3-dibenzolsulfonat
• CAS No.: 32905-27-4
• Molecular Formula: C₁₈H₁₃NO₉S₂
• Molecular Weight: 451.435
• Mol file: 32905-27-4.mol

Synonyms:

Chemical Property of 5-Nitropyrogallol-1,3-dibenzolsulfonat

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-Nitropyrogallol-1,3-dibenzolsulfonat

There total 1 articles about 5-Nitropyrogallol-1,3-dibenzolsulfonat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,6-bis-benzenesulfonyloxy-phenol (55020-69-4) → 5-Nitropyrogallol-1,3-dibenzolsulfonat (32905-27-4)

Guidance literature:

With nitric acid; acetic acid;

DOI:10.1039/j39710002577

Reference yield: 80.0%

5-Nitropyrogallol-1,3-dibenzolsulfonat (32905-27-4) → 5-amino-2-hydroxy-1,3-phenylene dibenzenesulfonate (1219498-96-0)

Guidance literature:

With iron; ammonium chloride; In water; acetone; Inert atmosphere; Reflux;

DOI:10.1080/00397910903009455

Reference yield:

5-Nitropyrogallol-1,3-dibenzolsulfonat (32905-27-4) → 3,4,5-trimethoxy-1-nitrobenzene (6307-90-0)

Guidance literature:

Multi-step reaction with 3 steps

2: aq. KOH / methanol

With potassium hydroxide; In methanol;

DOI:10.1039/j39710002577

upstream raw materials:

2,6-bis-benzenesulfonyloxy-phenol

Downstream raw materials:

5-Nitropyrogallol-1,3-dibenzolsulfonat-2-methylaether

5-Nitropyrogallol-1-benzolsulfonat

3,4,5-trimethoxy-1-nitrobenzene

3,4,5-trihydroxy-1-nitrobenzene