methylbis([[1-methyl-1-(di-p-tolylphosphino)ethyl]-η(5)-cyclopentadienyl]-κ(2)-P,P')zirconium(IV) methyltris(pentafluorophenyl)borate

Base Information

Chemical Name:methylbis([[1-methyl-1-(di-p-tolylphosphino)ethyl]-η(5)-cyclopentadienyl]-κ(2)-P,P')zirconium(IV) methyltris(pentafluorophenyl)borate
CAS No.:198766-02-8
Molecular Formula:C₁₉H₃BF₁₅*C₄₅H₅₁P₂Zr
Molecular Weight:1272.09
Hs Code.:

methylbis([[1-methyl-1-(di-p-tolylphosphino)ethyl]-η(5)-cyclopentadienyl]-κ(2)-P,P')zirconium(IV) methyltris(pentafluorophenyl)borate

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Chemical Property of methylbis([[1-methyl-1-(di-p-tolylphosphino)ethyl]-η(5)-cyclopentadienyl]-κ(2)-P,P')zirconium(IV) methyltris(pentafluorophenyl)borate

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Technology Process of methylbis([[1-methyl-1-(di-p-tolylphosphino)ethyl]-η(5)-cyclopentadienyl]-κ(2)-P,P')zirconium(IV) methyltris(pentafluorophenyl)borate

There total 2 articles about methylbis([[1-methyl-1-(di-p-tolylphosphino)ethyl]-η(5)-cyclopentadienyl]-κ(2)-P,P')zirconium(IV) methyltris(pentafluorophenyl)borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 198765-97-8
bis[[1-methyl-1-(di-p-tolylphosphino)ethyl]cyclopentadienyl]dimethylzirconium

: 1109-15-5
tris(pentafluorophenyl)borate

: 198766-02-8
methylbis([[1-methyl-1-(di-p-tolylphosphino)ethyl]-η(5)-cyclopentadienyl]-κ(2)-P,P')zirconium(IV) methyltris(pentafluorophenyl)borate

Guidance literature:: In toluene; Ar-atmosphere; mixing equimolar amts., stirring for 1 h; concn., addn. of pentane, stirring for 1 h, collection (filtration), washing (pentane), drying (vac.); elem. anal.;
DOI:10.1021/om970573t

Reference yield:

: 1665-00-5
dichloromethane-d2

: 198765-97-8
bis[[1-methyl-1-(di-p-tolylphosphino)ethyl]cyclopentadienyl]dimethylzirconium

: 1109-15-5
tris(pentafluorophenyl)borate

: [bis([[1-methyl-1-(di-p-tolylphosphino)ethyl]-η(5)-cyclopentadienyl]-κ(2)-P,P')zirconium(IV)][methyltris(pentafluorophenyl)borate]2

: 198766-06-2
chlorobis([[1-methyl-1-(di-p-tolylphosphino)ethyl]-η(5)-cyclopentadienyl]-κ(2)-P,P')zirconium(IV) methyltris(pentafluorophenyl)borate

: 198766-02-8
methylbis([[1-methyl-1-(di-p-tolylphosphino)ethyl]-η(5)-cyclopentadienyl]-κ(2)-P,P')zirconium(IV) methyltris(pentafluorophenyl)borate

Guidance literature:: In dichloromethane-d2; Ar-atmosphere; 2 equivs. of B(C6F5)3, mixing at -78°C, warming (NMR-control); not sepd.; NMR spectroscopy; Kinetics;
DOI:10.1021/om970573t