allyl [(S)-5-amino-3-phenylpentyl]carbamate

Base Information

Chemical Name:allyl [(S)-5-amino-3-phenylpentyl]carbamate
CAS No.:1312362-89-2
Molecular Formula:C₁₅H₂₂N₂O₂
Molecular Weight:262.352
Hs Code.:

Synonyms:

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Chemical Property of allyl [(S)-5-amino-3-phenylpentyl]carbamate

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Technology Process of allyl [(S)-5-amino-3-phenylpentyl]carbamate

There total 4 articles about allyl [(S)-5-amino-3-phenylpentyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15022-08-9
diallylcarbonate

: 875255-80-4
3-phenylpentane-1,5-diamine

: allyl [(R)-5-amino-3-phenylpentyl]carbamate

: 1312362-89-2
allyl [(S)-5-amino-3-phenylpentyl]carbamate

Guidance literature:: With pseudomonas cepacia lipase type I; In 1,4-dioxane; at 30 ℃; for 72h; optical yield given as %ee; Inert atmosphere; Enzymatic reaction;
DOI:10.1021/jo2007972

Reference yield:

: 1312362-88-1
3-phenylpentane-1,5-diazide

: allyl [(R)-5-amino-3-phenylpentyl]carbamate

: 1312362-89-2
allyl [(S)-5-amino-3-phenylpentyl]carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: water; triphenylphosphine / methanol / 14 h / 70 °C

2: pseudomonas cepacia lipase type I / 1,4-dioxane / 72 h / 30 °C / Inert atmosphere; Enzymatic reaction

With pseudomonas cepacia lipase type I; water; triphenylphosphine; In 1,4-dioxane; methanol;
DOI:10.1021/jo2007972

Reference yield:

: 829-27-6
3-phenylpentane-1,5-diol

: allyl [(R)-5-amino-3-phenylpentyl]carbamate

: 1312362-89-2
allyl [(S)-5-amino-3-phenylpentyl]carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / dichloromethane / 0 - 20 °C

2: sodium azide / N,N-dimethyl-formamide / 14 h / 55 °C / Inert atmosphere

3: water; triphenylphosphine / methanol / 14 h / 70 °C

4: pseudomonas cepacia lipase type I / 1,4-dioxane / 72 h / 30 °C / Inert atmosphere; Enzymatic reaction

With pyridine; sodium azide; pseudomonas cepacia lipase type I; water; triphenylphosphine; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo2007972