C₄₈H₆₉ClN₄O₅

Base Information

Chemical Name:C₄₈H₆₉ClN₄O₅
CAS No.:1449796-59-1
Molecular Formula:C₄₈H₆₉ClN₄O₅
Molecular Weight:817.553
Hs Code.:

C<sub>48</sub>H<sub>69</sub>ClN<sub>4</sub>O<sub>5</sub>

Synonyms:

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Chemical Property of C₄₈H₆₉ClN₄O₅

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Technology Process of C₄₈H₆₉ClN₄O₅

There total 17 articles about C₄₈H₆₉ClN₄O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1443467-40-0
(3aR,5aR,5bR,7aR,9S,11aR,11bR,13aS)-1-isopropyl-5a,5b,8,8,11a-pentamethyl-3a-(2-nitroethyl)-2-oxo-3,3a,4,5,5a,5b,6,7,7a,8,9,10,11,11a,11b,12,13,13a-octadecahydro-2H-cyclopenta[a]chrysen-9-yl acetate

: 1449796-59-1
C₄₈H₆₉ClN₄O₅

Guidance literature:: Multi-step reaction with 7 steps

1: acetic acid; sodium nitrite / dimethyl sulfoxide / 20 °C

2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C

3: hydrazine hydrate / dichloromethane / 0.5 h / 0 °C

4: acetic acid; silver benzoate / dichloromethane / 48 h / 20 °C

5: sodium hydroxide; water / tetrahydrofuran; methanol / 3 h / 20 °C

6: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

7: trifluoroacetic acid / dichloromethane / 20 °C

With dmap; oxalyl dichloride; water; silver benzoate; hydrazine hydrate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N,N-dimethyl-formamide; trifluoroacetic acid; sodium hydroxide; sodium nitrite; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide;

Reference yield:

: 1449796-76-2
2-((3aS,5aR,5bR,7aR,9S,11aR,11bR,13aS)-9-acetoxy-1-isopropyl-5a,5b,8,8,11a-pentamethyl-2-oxo-2,3,4,5,5a,5b,6,7,7a,8,9,10,11,11a,11b,12,13,13a-octadecahydro-3aH-cyclopenta[a]chrysen-3a-yl)acetic acid

: 1449796-59-1
C₄₈H₆₉ClN₄O₅

Guidance literature:: Multi-step reaction with 6 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C

2: hydrazine hydrate / dichloromethane / 0.5 h / 0 °C

3: acetic acid; silver benzoate / dichloromethane / 48 h / 20 °C

4: sodium hydroxide; water / tetrahydrofuran; methanol / 3 h / 20 °C

5: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

6: trifluoroacetic acid / dichloromethane / 20 °C

With dmap; oxalyl dichloride; water; silver benzoate; hydrazine hydrate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N,N-dimethyl-formamide; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 74-11-3
para-chlorobenzoic acid

: 1449796-59-1
C₄₈H₆₉ClN₄O₅

Guidance literature:: Multi-step reaction with 7 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 20 °C

2: triethylamine / dichloromethane / 0.5 h / 0 °C

3: Lawessons reagent / toluene / 3 h / Reflux

4: acetic acid; silver benzoate / dichloromethane / 48 h / 20 °C

5: sodium hydroxide; water / tetrahydrofuran; methanol / 3 h / 20 °C

6: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

7: trifluoroacetic acid / dichloromethane / 20 °C

With Lawessons reagent; dmap; oxalyl dichloride; water; silver benzoate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N,N-dimethyl-formamide; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; toluene;