C₁₈H₂₄BrNO₄S

Base Information

Chemical Name:C₁₈H₂₄BrNO₄S
CAS No.:1567388-45-7
Molecular Formula:C₁₈H₂₄BrNO₄S
Molecular Weight:430.363
Hs Code.:

C<sub>18</sub>H<sub>24</sub>BrNO<sub>4</sub>S

Synonyms:

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Chemical Property of C₁₈H₂₄BrNO₄S

Chemical Property:

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Technology Process of C₁₈H₂₄BrNO₄S

There total 7 articles about C₁₈H₂₄BrNO₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₀H₁₇N

: 51072-64-1
2-bromo-4,5-dimethoxybenzene-1-sulfonyl chloride

: 1567388-45-7
C₁₈H₂₄BrNO₄S

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1016/j.tetlet.2014.01.039

Reference yield:

: 5989-27-5,555-08-8,8022-90-0,9003-73-0,95327-98-3
D-limonene

: 1567388-45-7
C₁₈H₂₄BrNO₄S

Guidance literature:: Multi-step reaction with 7 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C

2.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C

3.1: pyridine / dichloromethane / 0 - 20 °C

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 15 h / 110 °C / Inert atmosphere; Sealed tube

4.2: 20 °C

5.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / 20 °C

5.2: 110 °C

6.1: sodium hydroxide / ethanol; water / 20 °C

7.1: triethylamine / dichloromethane / 0 - 20 °C

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; ethanol; dichloromethane; water; 5.1: |Overman Rearrangement / 5.2: |Overman Rearrangement;
DOI:10.1016/j.tetlet.2014.01.039

Reference yield:

: 216655-61-7
(5R)-2-methylene-5-(1-methylethenyl)-1-cyclohexanol

: 1567388-45-7
C₁₈H₂₄BrNO₄S

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridine / dichloromethane / 0 - 20 °C

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 15 h / 110 °C / Inert atmosphere; Sealed tube

2.2: 20 °C

3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / 20 °C

3.2: 110 °C

4.1: sodium hydroxide / ethanol; water / 20 °C

5.1: triethylamine / dichloromethane / 0 - 20 °C

With pyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water; 3.1: |Overman Rearrangement / 3.2: |Overman Rearrangement;
DOI:10.1016/j.tetlet.2014.01.039