C₂₇H₃₂N₂O₅S₂

Base Information

Chemical Name:C₂₇H₃₂N₂O₅S₂
CAS No.:1059104-00-5
Molecular Formula:C₂₇H₃₂N₂O₅S₂
Molecular Weight:528.693
Hs Code.:

C<sub>27</sub>H<sub>32</sub>N<sub>2</sub>O<sub>5</sub>S<sub>2</sub>

Synonyms:

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Chemical Property of C₂₇H₃₂N₂O₅S₂

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Technology Process of C₂₇H₃₂N₂O₅S₂

There total 3 articles about C₂₇H₃₂N₂O₅S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 146013-28-7
N-(tert-butyl)-5-isobutylthiophene-2-sulphonamide

: 1059104-00-5
C₂₇H₃₂N₂O₅S₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 4 h / -78 - -30 °C / Inert atmosphere

1.2: -40 - 20 °C / Inert atmosphere

2.1: hydrogenchloride / tetrahydrofuran; hexane; water / 0 °C / pH 2

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,2-dimethoxyethane; ethanol; water / Microwave irradiation

4.1: boron trichloride / dichloromethane

5.1: triethylamine / dichloromethane

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; boron trichloride; sodium carbonate; triethylamine; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; hexane; dichloromethane; water; 3.1: Suzuki coupling;
DOI:10.1002/jlcr.1793

Reference yield:

: 163520-14-7
5-isobutyl-2 -(tert-butylaminosulfonyl)-3-thiopheneboronic acid

: 1059104-00-5
C₂₇H₃₂N₂O₅S₂

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,2-dimethoxyethane; ethanol; water / Microwave irradiation

2: boron trichloride / dichloromethane

3: triethylamine / dichloromethane

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; boron trichloride; sodium carbonate; triethylamine; In 1,2-dimethoxyethane; ethanol; dichloromethane; water; 1: Suzuki coupling;
DOI:10.1002/jlcr.1793