Technology Process of C55H48N4O5
There total 6 articles about C55H48N4O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
2: 78 percent / p-TozOH / various solvent(s) / 0.33 h / Heating
3: 90 percent / LiAlH4 / diethyl ether / 1 h addition then 2 h room t.
4: 94 percent / water / 6 M H2SO4 / acetone / 1.5 h / Heating
5: 86 percent / 66 percent aq. HBr / 4 h / Heating
6: K2CO3 / dimethylformamide / addition 4 h, 100 deg C, then 4 h, 100 deg C
With
lithium aluminium tetrahydride; water; hydrogen bromide; potassium carbonate;
sulfuric acid; toluene-4-sulfonic acid;
In
diethyl ether; N,N-dimethyl-formamide; acetone;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 78 percent / p-TozOH / various solvent(s) / 0.33 h / Heating
2: 90 percent / LiAlH4 / diethyl ether / 1 h addition then 2 h room t.
3: 94 percent / water / 6 M H2SO4 / acetone / 1.5 h / Heating
4: 86 percent / 66 percent aq. HBr / 4 h / Heating
5: K2CO3 / dimethylformamide / addition 4 h, 100 deg C, then 4 h, 100 deg C
With
lithium aluminium tetrahydride; water; hydrogen bromide; potassium carbonate;
sulfuric acid; toluene-4-sulfonic acid;
In
diethyl ether; N,N-dimethyl-formamide; acetone;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 94 percent / water / 6 M H2SO4 / acetone / 1.5 h / Heating
2: 86 percent / 66 percent aq. HBr / 4 h / Heating
3: K2CO3 / dimethylformamide / addition 4 h, 100 deg C, then 4 h, 100 deg C
With
water; hydrogen bromide; potassium carbonate;
sulfuric acid;
In
N,N-dimethyl-formamide; acetone;
