trichlorobis(ethyldiphenylphosphine oxide)nitrosylmolybdenum

Base Information

Chemical Name:trichlorobis(ethyldiphenylphosphine oxide)nitrosylmolybdenum
CAS No.:63280-63-7
Molecular Formula:C₂₈H₃₀Cl₃MoNO₃P₂
Molecular Weight:692.798
Hs Code.:

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Chemical Property of trichlorobis(ethyldiphenylphosphine oxide)nitrosylmolybdenum

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Technology Process of trichlorobis(ethyldiphenylphosphine oxide)nitrosylmolybdenum

There total 2 articles about trichlorobis(ethyldiphenylphosphine oxide)nitrosylmolybdenum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 10102-43-9
nitrogen(II) oxide

: 10241-05-1
molybdenum(V) chloride

: 1733-57-9
ethydiphenylphosphine oxide

: 63280-63-7
trichlorobis(ethyldiphenylphosphine oxide)nitrosylmolybdenum

Guidance literature:: In benzene; N2-atmosphere; passing NO2 through soln. of MoCl5 (room temp., stirring,8 min), removal of NO (vac.), filtration, washing (benzene), drying (0. 01 Torr), suspending in C6H6, addn. of OPMePh2, stirring (room temp., 30min); filtration, crystn. on refrigeration;
DOI:10.1039/DT9770000429

Reference yield:

: 30059-52-0
tetrachlorobis(ethyldiphenylphosphine)molybdenum(IV)

: 10102-43-9
nitrogen(II) oxide

: 63280-63-7
trichlorobis(ethyldiphenylphosphine oxide)nitrosylmolybdenum

: 15227-59-5
dichlorobis(ethyldiphenylphosphine oxide)dinitrosylmolybdenum

Guidance literature:: In tetrahydrofuran; N2-atmosphere; passing NO through soln. of Mo-complex (room temp., 2 min, stirring); evapn. (reduced pressure), washing (benzene), repeated recrystn. (CH2Cl2/hexane); product mixt. not fully sepd., detd. by IR spectroscopy;
DOI:10.1039/DT9770000429