cis-1-Acetamido-2-cyclohexen-4-ylacetat

Base Information

Chemical Name:cis-1-Acetamido-2-cyclohexen-4-ylacetat
CAS No.:77803-78-2
Molecular Formula:C₁₀H₁₅NO₃
Molecular Weight:197.234
Hs Code.:

Synonyms:

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Chemical Property of cis-1-Acetamido-2-cyclohexen-4-ylacetat

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Technology Process of cis-1-Acetamido-2-cyclohexen-4-ylacetat

There total 3 articles about cis-1-Acetamido-2-cyclohexen-4-ylacetat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 108-24-7
acetic anhydride

: 77803-77-1,96093-87-7,131321-46-5
(1S*,4R*)-4-aminocyclohex-2-enol

: 77803-78-2,109856-86-2,123808-79-7
cis-1-Acetamido-2-cyclohexen-4-ylacetat

Guidance literature:: In pyridine; overnight;

Reference yield:

: 56239-25-9
2-Oxa-3-azabicyclo<2.2.2>oct-5-ene hydrochloride

: 77803-78-2,109856-86-2,123808-79-7
cis-1-Acetamido-2-cyclohexen-4-ylacetat

Guidance literature:: Multi-step reaction with 2 steps

1: H₂, methylviologen / Methanosarcina barkeri DSM 800 / 36 °C / pH 7.0; further bacteria

2: pyridine

With hydrogen; paraquat dichloride; Methanosarcina barkeri DSM 800; In pyridine;
DOI:10.1016/S0040-4039(00)96179-3

Reference yield:

: 56239-25-9
(+/-)-2-Oxa-3-azabicyclo[2.2.2]oct-5-ene hydrochloride

: 77803-78-2,109856-86-2,123808-79-7
cis-1-Acetamido-2-cyclohexen-4-ylacetat

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / Zn, conc. HCl / H₂O / 8 h / 0 - 10 °C

2: 92 percent / pyridine / overnight

With hydrogenchloride; zinc; In pyridine; water;