1-[1-(Trichlorosilyl)cyclohexyl]piperidine

Base Information

Chemical Name:1-[1-(Trichlorosilyl)cyclohexyl]piperidine
CAS No.:105867-11-6
Molecular Formula:C11H20Cl3NSi
Molecular Weight:300.731
Hs Code.:
DSSTox Substance ID:DTXSID40544074
Wikidata:Q82421052

Synonyms:105867-11-6;1-[1-(Trichlorosilyl)cyclohexyl]piperidine;DTXSID40544074

Suppliers and Price of 1-[1-(Trichlorosilyl)cyclohexyl]piperidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 1-[1-(Trichlorosilyl)cyclohexyl]piperidine

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:299.043059
Heavy Atom Count:16
Complexity:230

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC(CC1)(N2CCCCC2)[Si](Cl)(Cl)Cl

Technology Process of 1-[1-(Trichlorosilyl)cyclohexyl]piperidine

There total 3 articles about 1-[1-(Trichlorosilyl)cyclohexyl]piperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 2981-10-4
1-(cyclohex-1-en-1-yl)piperidine

: 105867-11-6
N-(1-trichlorosilylcyclohexyl)piperidine

Guidance literature:: With trichlorosilane; In acetonitrile; for 2.5h; Heating; var.: without solvent;
DOI:10.1016/0022-328X(86)80004-3

Reference yield:

: 110-89-4
piperidine

: 105867-11-6
N-(1-trichlorosilylcyclohexyl)piperidine

Guidance literature:: Multi-step reaction with 2 steps

1: H₂SO₄ / benzene / Heating; H₂O was collected as the benzene azeotrope

2: 77 percent / trichlorosilane / acetonitrile / 2.5 h / Heating; var.: without solvent

With sulfuric acid; trichlorosilane; In acetonitrile; benzene;
DOI:10.1016/0022-328X(86)80004-3

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 105867-11-6
N-(1-trichlorosilylcyclohexyl)piperidine

Guidance literature:: Multi-step reaction with 2 steps

1: H₂SO₄ / benzene / Heating; H₂O was collected as the benzene azeotrope

2: 77 percent / trichlorosilane / acetonitrile / 2.5 h / Heating; var.: without solvent

With sulfuric acid; trichlorosilane; In acetonitrile; benzene;
DOI:10.1016/0022-328X(86)80004-3