Technology Process of tetrabutylammonium 6-mesityl-2-picolinate
There total 5 articles about tetrabutylammonium 6-mesityl-2-picolinate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetra(n-butyl)ammonium hydroxide;
In
dichloromethane; water;
for 1h;
Inert atmosphere;
DOI:10.1039/c2dt30585b
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tris-(dibenzylideneacetone)dipalladium(0); potassium phosphate; tricyclohexylphosphine / toluene / 24 h / 100 °C / Inert atmosphere
2: sodium hydroxide / methanol; diethyl ether / 1 h / Inert atmosphere
3: hydrogenchloride / water; acetone / 0.67 h / Inert atmosphere; Sonication
4: tetra(n-butyl)ammonium hydroxide / dichloromethane; water / 1 h / Inert atmosphere
With
hydrogenchloride; potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); tetra(n-butyl)ammonium hydroxide; sodium hydroxide; tricyclohexylphosphine;
In
methanol; diethyl ether; dichloromethane; water; acetone; toluene;
1: Suzuki-Miyaura cross-coupling;
DOI:10.1039/c2dt30585b
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydroxide / methanol; diethyl ether / 1 h / Inert atmosphere
2: hydrogenchloride / water; acetone / 0.67 h / Inert atmosphere; Sonication
3: tetra(n-butyl)ammonium hydroxide / dichloromethane; water / 1 h / Inert atmosphere
With
hydrogenchloride; tetra(n-butyl)ammonium hydroxide; sodium hydroxide;
In
methanol; diethyl ether; dichloromethane; water; acetone;
DOI:10.1039/c2dt30585b
