C₅₀H₈₁NO₁₁

Base Information

• Chemical Name: C₅₀H₈₁NO₁₁
• CAS No.: 1621861-48-0
• Molecular Formula: C₅₀H₈₁NO₁₁
• Molecular Weight: 872.193
• Mol file: 1621861-48-0.mol

Synonyms:

Chemical Property of C₅₀H₈₁NO₁₁

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₀H₈₁NO₁₁

There total 4 articles about C₅₀H₈₁NO₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C26H34O4 + 2-amino-1-O-(α-D-galactopyranosyl)-1,3,4-octadecanetriol (223748-98-9) → C50H81NO11 (1621861-48-0)

Guidance literature:

C₂₆H₃₄O₄; With oxalyl dichloride; at 60 ℃; for 2h;

2-amino-1-O-(α-D-galactopyranosyl)-1,3,4-octadecanetriol; With sodium acetate; In tetrahydrofuran; at 20 ℃; for 12h;

DOI:10.1021/acs.bioconjchem.8b00484

Reference yield:

3-benzoylbenzyl bromide (22071-24-5) → C50H81NO11 (1621861-48-0)

Guidance literature:

Multi-step reaction with 3 steps

1.1: calcium carbonate / tetrahydrofuran; water / 12 h / 100 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C

3.1: oxalyl dichloride / 2 h / 60 °C

3.2: 12 h / 20 °C

With oxalyl dichloride; sodium hydride; calcium carbonate; In tetrahydrofuran; water; N,N-dimethyl-formamide;

DOI:10.1021/acs.bioconjchem.8b00484

Reference yield:

[3-(hydroxymethyl)phenyl](phenyl)methanone (56338-25-1) → C50H81NO11 (1621861-48-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C

2.1: oxalyl dichloride / 2 h / 60 °C

2.2: 12 h / 20 °C

With oxalyl dichloride; sodium hydride; In N,N-dimethyl-formamide;

DOI:10.1021/acs.bioconjchem.8b00484

upstream raw materials:

3-benzoylbenzyl bromide

2-amino-1-O-(α-D-galactopyranosyl)-1,3,4-octadecanetriol

[3-(hydroxymethyl)phenyl](phenyl)methanone

Refernces

• 1、 -. "MODIFIED GLYCOLIPIDS AND METHODS OF MAKING AND USING THE SAME". Paragraph 0383. . Retrieved 2014/08/19.