C₄₅H₄₃BN₄O₁₁

Base Information

Chemical Name:C₄₅H₄₃BN₄O₁₁
CAS No.:1425051-98-4
Molecular Formula:C₄₅H₄₃BN₄O₁₁
Molecular Weight:826.668
Hs Code.:

C<sub>45</sub>H<sub>43</sub>BN<sub>4</sub>O<sub>11</sub>

Synonyms:

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Chemical Property of C₄₅H₄₃BN₄O₁₁

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Technology Process of C₄₅H₄₃BN₄O₁₁

There total 11 articles about C₄₅H₄₃BN₄O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1425051-97-3
C₃₈H₃₉BN₂O₈

: 100-28-7
4-Nitrophenyl isocyanate

: 1425051-98-4
C₄₅H₄₃BN₄O₁₁

Guidance literature:: With triethylamine; In tetrahydrofuran; at 23 ℃; for 1.5h; Inert atmosphere;
DOI:10.1021/jo400105m

Reference yield:

: 1425052-06-7
C₁₈H₂₄O₂Si

: 1425051-98-4
C₄₅H₄₃BN₄O₁₁

Guidance literature:: Multi-step reaction with 6 steps

1.1: toluene-4-sulfonic acid / tetrahydrofuran; water / 14 h / 23 °C / Inert atmosphere

2.1: diphenylphosphoranyl azide; triethylamine / benzene / 1 h / 85 °C / Inert atmosphere

2.2: 3 h / 85 °C / Inert atmosphere

3.1: sodium dihydrogen phosphate monohydrate; sodium chlorite; 2-methyl-but-2-ene / water; acetone / 0.5 h / 23 °C / Inert atmosphere

4.1: diphenylphosphoranyl azide; triethylamine / benzene / 1 h / 85 °C / Inert atmosphere

4.2: 3 h / 85 °C / Inert atmosphere

5.1: toluene-4-sulfonic acid / tetrahydrofuran; water / 14 h / 23 °C / Inert atmosphere

5.2: 24 h / 23 °C / Inert atmosphere

6.1: triethylamine / tetrahydrofuran / 1.5 h / 23 °C / Inert atmosphere

With sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; diphenylphosphoranyl azide; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; water; acetone; benzene; 2.1: |Curtius Rearrangement / 2.2: |Curtius Rearrangement / 4.1: |Curtius Rearrangement / 4.2: |Curtius Rearrangement;
DOI:10.1021/jo400105m

Reference yield:

: 79996-99-9
1-bromo-4-bromomethyl-naphthalene

: 1425051-98-4
C₄₅H₄₃BN₄O₁₁

Guidance literature:: Multi-step reaction with 9 steps

1.1: calcium carbonate / water; 1,4-dioxane / 12 h / 110 °C / Inert atmosphere

2.1: dmap; 1H-imidazole / dichloromethane / 16 h / 23 °C / Inert atmosphere

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.08 h / -78 °C / Inert atmosphere

3.2: 1.5 h / -78 - 23 °C / Inert atmosphere

4.1: toluene-4-sulfonic acid / tetrahydrofuran; water / 14 h / 23 °C / Inert atmosphere

5.1: diphenylphosphoranyl azide; triethylamine / benzene / 1 h / 85 °C / Inert atmosphere

5.2: 3 h / 85 °C / Inert atmosphere

6.1: sodium dihydrogen phosphate monohydrate; sodium chlorite; 2-methyl-but-2-ene / water; acetone / 0.5 h / 23 °C / Inert atmosphere

7.1: diphenylphosphoranyl azide; triethylamine / benzene / 1 h / 85 °C / Inert atmosphere

7.2: 3 h / 85 °C / Inert atmosphere

8.1: toluene-4-sulfonic acid / tetrahydrofuran; water / 14 h / 23 °C / Inert atmosphere

8.2: 24 h / 23 °C / Inert atmosphere

9.1: triethylamine / tetrahydrofuran / 1.5 h / 23 °C / Inert atmosphere

With 1H-imidazole; dmap; sodium chlorite; n-butyllithium; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; diphenylphosphoranyl azide; toluene-4-sulfonic acid; triethylamine; calcium carbonate; In tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; water; acetone; benzene; 5.1: |Curtius Rearrangement / 5.2: |Curtius Rearrangement / 7.1: |Curtius Rearrangement / 7.2: |Curtius Rearrangement;
DOI:10.1021/jo400105m