n-butyl N-benzyloxycarbonylvalinoate

Base Information

• Chemical Name: n-butyl N-benzyloxycarbonylvalinoate
• CAS No.: 174872-56-1
• Molecular Formula: C₁₇H₂₅NO₄
• Molecular Weight: 307.39

Synonyms:

Chemical Property of n-butyl N-benzyloxycarbonylvalinoate

Chemical Property:

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Technology Process of n-butyl N-benzyloxycarbonylvalinoate

There total 2 articles about n-butyl N-benzyloxycarbonylvalinoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

methyl (2S)-3-methyl-[(benzyloxy)carbonylamino]butanoate (24210-19-3) + butan-1-ol (71-36-3) → n-butyl N-benzyloxycarbonylvalinoate (174872-56-1)

Guidance literature:

With dmap; C₁₂H₆F₁₈O₁₃Zn₄; In di-isopropyl ether; for 18h; Reflux; Inert atmosphere;

DOI:10.1055/s-0031-1290096

Reference yield: 93.0%

→ n-butyl N-benzyloxycarbonylvalinoate (174872-56-1)

Guidance literature:

With oxo[hexa(trifluoroacetato)]tetrazinc; C₁₉H₂₄N₄O; In di-isopropyl ether; for 18h; Reflux;

upstream raw materials:

methyl (2S)-3-methyl-[(benzyloxy)carbonylamino]butanoate

butan-1-ol

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