C₃₃H₃₈N₄O₇S

Base Information

Chemical Name:C₃₃H₃₈N₄O₇S
CAS No.:957468-63-2
Molecular Formula:C₃₃H₃₈N₄O₇S
Molecular Weight:634.753
Hs Code.:

C<sub>33</sub>H<sub>38</sub>N<sub>4</sub>O<sub>7</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₃₈N₄O₇S

Chemical Property:

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Technology Process of C₃₃H₃₈N₄O₇S

There total 6 articles about C₃₃H₃₈N₄O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Phenylmethyl [2R-hydroxy-3-[(2-methylpropyl)(4-acetamidophenylsulfonyl)amino]-1S-(phenylmethyl)propyl]carbamate

: 957468-63-2
C₃₃H₃₈N₄O₇S

Guidance literature:: Multi-step reaction with 2 steps

1: 10% palladium on activated charcoal; ammonium formate / methanol

2: 4-methyl-morpholine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / acetonitrile / Inert atmosphere

With 4-methyl-morpholine; 10% palladium on activated charcoal; ammonium formate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; In methanol; acetonitrile;
DOI:10.1111/j.1747-0285.2010.00995.x

Reference yield:

: 1161-13-3
N-Cbz-L-Phe

: 957468-63-2
C₃₃H₃₈N₄O₇S

Guidance literature:: Multi-step reaction with 7 steps

1.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / -20 °C

1.2: -20 °C

2.1: hydrogenchloride / diethyl ether / -20 °C

3.1: lithium tri-t-butoxyaluminum hydride / ethanol / -78 °C

4.1: isopropyl alcohol / 70 °C

5.1: sodium hydrogencarbonate / water; 1,2-dichloro-ethane

6.1: 10% palladium on activated charcoal; ammonium formate / methanol

7.1: 4-methyl-morpholine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / acetonitrile / Inert atmosphere

With 4-methyl-morpholine; hydrogenchloride; 10% palladium on activated charcoal; ammonium formate; sodium hydrogencarbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; lithium tri-t-butoxyaluminum hydride; isobutyl chloroformate; In tetrahydrofuran; methanol; diethyl ether; ethanol; water; 1,2-dichloro-ethane; isopropyl alcohol; acetonitrile;
DOI:10.1111/j.1747-0285.2010.00995.x

Reference yield:

: 15196-02-8
(S)-3-[(benzyloxycarbonyl)amino]-1-diazo-4-phenyl-2-butanone

: 957468-63-2
C₃₃H₃₈N₄O₇S

Guidance literature:: Multi-step reaction with 6 steps

1: hydrogenchloride / diethyl ether / -20 °C

2: lithium tri-t-butoxyaluminum hydride / ethanol / -78 °C

3: isopropyl alcohol / 70 °C

4: sodium hydrogencarbonate / water; 1,2-dichloro-ethane

5: 10% palladium on activated charcoal; ammonium formate / methanol

6: 4-methyl-morpholine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / acetonitrile / Inert atmosphere

With 4-methyl-morpholine; hydrogenchloride; 10% palladium on activated charcoal; ammonium formate; sodium hydrogencarbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; lithium tri-t-butoxyaluminum hydride; In methanol; diethyl ether; ethanol; water; 1,2-dichloro-ethane; isopropyl alcohol; acetonitrile;
DOI:10.1111/j.1747-0285.2010.00995.x