C₃₄H₃₆N₆O₅

Base Information

Chemical Name:C₃₄H₃₆N₆O₅
CAS No.:1448424-60-9
Molecular Formula:C₃₄H₃₆N₆O₅
Molecular Weight:608.697
Hs Code.:

C<sub>34</sub>H<sub>36</sub>N<sub>6</sub>O<sub>5</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₄H₃₆N₆O₅

Chemical Property:

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Technology Process of C₃₄H₃₆N₆O₅

There total 3 articles about C₃₄H₃₆N₆O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 29022-11-5
N-(fluoren-9-ylmethoxycarbonyl)glycine

: 35661-39-3,136132-75-7
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine

: 1268831-55-5
(S)-2- ((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-(2-(p-tolyl)-1H-indol-3-yl)propanoic acid

: 35737-15-6
Fmoc-Trp-OH

: 1448424-60-9
C₃₄H₃₆N₆O₅

Guidance literature:: Fmoc-Trp-OH; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 0.833333h; 2-chlorotrityl chloride resin Inert atmosphere;

With piperidine; In N,N-dimethyl-formamide; at 20 ℃; for 0.183333h; 2-chlorotrityl chloride resin Inert atmosphere;

N-(fluoren-9-ylmethoxycarbonyl)glycine; N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine; (S)-2- ((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-(2-(p-tolyl)-1H-indol-3-yl)propanoic acid; Further stages;
DOI:10.1021/jo400961x

Reference yield:

: 624-31-7
4-tolyl iodide

: 1448424-60-9
C₃₄H₃₆N₆O₅

Guidance literature:: Multi-step reaction with 2 steps

1.1: silver tetrafluoroborate; trifluoroacetic acid; palladium diacetate / N,N-dimethyl-formamide / 0.33 h / 90 °C / Inert atmosphere; Microwave irradiation; Sealed tube

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.83 h / 20 °C / Inert atmosphere

2.2: 0.18 h / 20 °C / Inert atmosphere

With silver tetrafluoroborate; palladium diacetate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo400961x

Reference yield:

: 35737-15-6
Fmoc-Trp-OH

: 1448424-60-9
C₃₄H₃₆N₆O₅

Guidance literature:: Multi-step reaction with 2 steps

1.1: silver tetrafluoroborate; trifluoroacetic acid; palladium diacetate / N,N-dimethyl-formamide / 0.33 h / 90 °C / Inert atmosphere; Microwave irradiation; Sealed tube

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.83 h / 20 °C / Inert atmosphere

2.2: 0.18 h / 20 °C / Inert atmosphere

With silver tetrafluoroborate; palladium diacetate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo400961x