Technology Process of C24H14BrN3O2
There total 4 articles about C24H14BrN3O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium carbonate / acetone / 24 h / Reflux
1.2: 90 °C
2.1: sodium carbonate / toluene / Reflux
3.1: ammonium acetate / 140 °C
4.1: copper diacetate; pyridine; oxygen; triethylamine / dichloromethane / 20 °C / Molecular sieve
With
pyridine; ammonium acetate; oxygen; copper diacetate; sodium carbonate; triethylamine;
In
dichloromethane; acetone; toluene;
DOI:10.1016/j.bmcl.2013.02.021
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium carbonate / toluene / Reflux
2: ammonium acetate / 140 °C
3: copper diacetate; pyridine; oxygen; triethylamine / dichloromethane / 20 °C / Molecular sieve
With
pyridine; ammonium acetate; oxygen; copper diacetate; sodium carbonate; triethylamine;
In
dichloromethane; toluene;
DOI:10.1016/j.bmcl.2013.02.021
- Guidance literature:
-
Multi-step reaction with 2 steps
1: ammonium acetate / 140 °C
2: copper diacetate; pyridine; oxygen; triethylamine / dichloromethane / 20 °C / Molecular sieve
With
pyridine; ammonium acetate; oxygen; copper diacetate; triethylamine;
In
dichloromethane;
DOI:10.1016/j.bmcl.2013.02.021