2,5-bis-(p-bromomethylphenylmethylthiomethyl)thiophen

Base Information

Chemical Name:2,5-bis-(p-bromomethylphenylmethylthiomethyl)thiophen
CAS No.:81509-60-6
Molecular Formula:C₂₂H₂₂Br₂S₃
Molecular Weight:542.423
Hs Code.:

Synonyms:

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Chemical Property of 2,5-bis-(p-bromomethylphenylmethylthiomethyl)thiophen

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Technology Process of 2,5-bis-(p-bromomethylphenylmethylthiomethyl)thiophen

There total 5 articles about 2,5-bis-(p-bromomethylphenylmethylthiomethyl)thiophen which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 81509-59-3
2,5-bis-(p-hydroxyphenylmethylthiomethyl)thiophen

: 81509-60-6
2,5-bis-(p-bromomethylphenylmethylthiomethyl)thiophen

Guidance literature:: With phosphorus tribromide; In benzene; for 1h;

Reference yield:

: 28569-48-4
2,5-bis-chloromethyl-thiophene

: 81509-60-6
2,5-bis-(p-bromomethylphenylmethylthiomethyl)thiophen

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) potassium hydroxide / 1.) methanol, 30 min, 2.) reflux, 12 h

2: 81 percent / borane-tetrahydrofuran complex / tetrahydrofuran / 2 h / Ambient temperature

3: 68 percent / phosphorus tribromide / benzene / 1 h

With potassium hydroxide; borane-THF; phosphorus tribromide; In tetrahydrofuran; benzene;

Reference yield:

: 6232-88-8
4-bromomethylbenzoic Acid

: 81509-60-6
2,5-bis-(p-bromomethylphenylmethylthiomethyl)thiophen

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) thiourea, 2.) sodium hydrogen carbonate / 1.) water, reflux, 1 h, 2.) reflux

2: 1.) potassium hydroxide / 1.) methanol, 30 min, 2.) reflux, 12 h

3: 81 percent / borane-tetrahydrofuran complex / tetrahydrofuran / 2 h / Ambient temperature

4: 68 percent / phosphorus tribromide / benzene / 1 h

With potassium hydroxide; borane-THF; phosphorus tribromide; sodium hydrogencarbonate; thiourea; In tetrahydrofuran; benzene;