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19-norcholest-5-en-3β-ol benzoate

Base Information Edit
  • Chemical Name:19-norcholest-5-en-3β-ol benzoate
  • CAS No.:83205-49-6
  • Molecular Formula:C33H48O2
  • Molecular Weight:476.743
  • Hs Code.:
  • Mol file:83205-49-6.mol
19-norcholest-5-en-3β-ol benzoate

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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of 19-norcholest-5-en-3β-ol benzoate Edit
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Technology Process of 19-norcholest-5-en-3β-ol benzoate

There total 7 articles about 19-norcholest-5-en-3β-ol benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 7 steps
1: 65 percent / NBS, 60percent HClO4 / diethyl ether; H2O / 3 h / Ambient temperature
2: 97 percent / Pb(OAc)4, CaCO3, I2 / cyclohexane / 1 h / Heating; Irradiation
3: 79 percent / Zn, CuCl / ethanol / 10 h / Heating
4: 84 percent / PCC / CH2Cl2 / 2 h / Ambient temperature
5: 38 percent / cyclohexane / 16 h / Irradiation
6: 80 percent / conc. NaOH / ethanol / 2 h / Heating
7: 69 percent / pyridine
With lead(IV) acetate; sodium hydroxide; N-Bromosuccinimide; perchloric acid; iodine; pyridinium chlorochromate; calcium carbonate; copper(l) chloride; zinc; In pyridine; diethyl ether; ethanol; dichloromethane; cyclohexane; water;
Guidance literature:
Multi-step reaction with 6 steps
1: 97 percent / Pb(OAc)4, CaCO3, I2 / cyclohexane / 1 h / Heating; Irradiation
2: 79 percent / Zn, CuCl / ethanol / 10 h / Heating
3: 84 percent / PCC / CH2Cl2 / 2 h / Ambient temperature
4: 38 percent / cyclohexane / 16 h / Irradiation
5: 80 percent / conc. NaOH / ethanol / 2 h / Heating
6: 69 percent / pyridine
With lead(IV) acetate; sodium hydroxide; iodine; pyridinium chlorochromate; calcium carbonate; copper(l) chloride; zinc; In pyridine; ethanol; dichloromethane; cyclohexane;
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