benzenesulfonic acid-[3-(3-methoxy-benzyl)-2,4,6-trimethyl-anilide]

Base Information

Chemical Name:benzenesulfonic acid-[3-(3-methoxy-benzyl)-2,4,6-trimethyl-anilide]
CAS No.:858502-74-6
Molecular Formula:C₂₃H₂₅NO₃S
Molecular Weight:395.522
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzenesulfonic acid-[3-(3-methoxy-benzyl)-2,4,6-trimethyl-anilide]

Chemical Property:

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Technology Process of benzenesulfonic acid-[3-(3-methoxy-benzyl)-2,4,6-trimethyl-anilide]

There total 6 articles about benzenesulfonic acid-[3-(3-methoxy-benzyl)-2,4,6-trimethyl-anilide] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 859331-00-3
3-(2,4,6-trimethyl-3-nitro-benzyl)-anisole

: 858502-74-6
benzenesulfonic acid-[3-(3-methoxy-benzyl)-2,4,6-trimethyl-anilide]

Guidance literature:: With nickel; hydrazine hydrate; anschliessenden Erhitzen mit Benzolsulfonylchlorid in wss.NaHCO₃;
DOI:10.1021/ja01584a038

Reference yield:

: 856192-10-4
mesityl-(3-nitro-phenyl)-methane

: 858502-74-6
benzenesulfonic acid-[3-(3-methoxy-benzyl)-2,4,6-trimethyl-anilide]

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid anhydride; acetic acid; HNO₃ / -15 °C

2: platinum; benzene / Hydrogenation

3: aqueous H₂SO₄ / Diazotization_.Erwaermen des Reaktionsprodukts mit wss. NaOH und Dimethylsulfat

4: N₂H_4.H₂O; Raney nickel / anschliessenden Erhitzen mit Benzolsulfonylchlorid in wss.NaHCO₃

With sulfuric acid; nitric acid; acetic anhydride; nickel; hydrazine hydrate; acetic acid; platinum; benzene;
DOI:10.1021/ja01584a038

Reference yield:

: 857007-63-7
3-(2,4,6-trimethyl-3-nitro-benzyl)-aniline

: 858502-74-6
benzenesulfonic acid-[3-(3-methoxy-benzyl)-2,4,6-trimethyl-anilide]

Guidance literature:: Multi-step reaction with 2 steps

1: aqueous H₂SO₄ / Diazotization_.Erwaermen des Reaktionsprodukts mit wss. NaOH und Dimethylsulfat

2: N₂H_4.H₂O; Raney nickel / anschliessenden Erhitzen mit Benzolsulfonylchlorid in wss.NaHCO₃

With sulfuric acid; nickel; hydrazine hydrate;
DOI:10.1021/ja01584a038