Benzamide, 2-bromo-N,N-diethyl-4,5-dimethoxy-

Base Information

Chemical Name:Benzamide, 2-bromo-N,N-diethyl-4,5-dimethoxy-
CAS No.:105875-33-0
Molecular Formula:C13H18BrNO3
Molecular Weight:316.195
Hs Code.:
DSSTox Substance ID:DTXSID10466673

Synonyms:105875-33-0;Benzamide, 2-bromo-N,N-diethyl-4,5-dimethoxy-;SCHEMBL2336464;DTXSID10466673;FT-0734402

Suppliers and Price of Benzamide, 2-bromo-N,N-diethyl-4,5-dimethoxy-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Benzamide, 2-bromo-N,N-diethyl-4,5-dimethoxy-

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:315.04701
Heavy Atom Count:18
Complexity:271

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)C(=O)C1=CC(=C(C=C1Br)OC)OC

Technology Process of Benzamide, 2-bromo-N,N-diethyl-4,5-dimethoxy-

There total 2 articles about Benzamide, 2-bromo-N,N-diethyl-4,5-dimethoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6286-46-0
2-bromo-4,5-dimethoxybenzoic acid

: 105875-33-0
2-bromo-N,N-diethyl-4,5-dimethoxy-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / N,N-dimethyl-formamide / 1 h / Reflux

2: potassium hydroxide / water; dichloromethane / 1.5 h / 0 °C

With thionyl chloride; potassium hydroxide; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tetasy.2015.01.002

Reference yield:

: 105875-33-0
2-bromo-N,N-diethyl-4,5-dimethoxy-benzamide

Guidance literature:

Reference yield: 53.0%

: 90-04-0
2-methoxy-phenylamine

: 105875-33-0
2-bromo-N,N-diethyl-4,5-dimethoxy-benzamide

: 207802-69-5
N,N-diethyl-4,5-dimethoxy-2-(2-methoxyanilino)benzamide

Guidance literature:: With sodium t-butanolate; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In toluene; at 90 - 100 ℃;
DOI:10.1055/s-1998-1654