[Co2Pd(μ3-CO)(CO)4(μ-bis(diphenylphosphino)methane)2]

Base Information

Chemical Name:[Co2Pd(μ3-CO)(CO)4(μ-bis(diphenylphosphino)methane)2]
CAS No.:113109-25-4
Molecular Formula:C₅₅H₄₄Co₂O₅P₄Pd
Molecular Weight:1133.25
Hs Code.:

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Chemical Property of [Co2Pd(μ3-CO)(CO)4(μ-bis(diphenylphosphino)methane)2]

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Technology Process of [Co2Pd(μ3-CO)(CO)4(μ-bis(diphenylphosphino)methane)2]

There total 7 articles about [Co2Pd(μ3-CO)(CO)4(μ-bis(diphenylphosphino)methane)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 113109-24-3
{Pd₂Co₂(CO)7(dppm)2}

: 113109-25-4
[Co2Pd(μ3-CO)(CO)4(μ-bis(diphenylphosphino)methane)2]

Guidance literature:: In toluene; A soln. of {Pd2Co2(CO)7(dppm)2} in toluene was heated to 60-80°C and stirred for 24 h.; The react. mixt. was filtered to remove insol. brown material and evapd. to dryness, affording the red-brown solid, which was recrystd. from toluene/n-hexane. Elem.anal.;

Reference yield: 35.0%

: 15617-18-2,39958-10-6,14220-64-5
bis(benzonitrile)palladium(II) dichloride

: 14878-28-5
sodium tetracarbonyl cobaltate

: 2071-20-7
bis-diphenylphosphinomethane

: 38425-01-3
(bis(diphenylphosphino)methane)palladium(II) dichloride

: 113109-25-4
[Co2Pd(μ3-CO)(CO)4(μ-bis(diphenylphosphino)methane)2]

Guidance literature:: In tetrahydrofuran; byproducts: NaCl, CO, PhCN; (N2), filtered soln. of Na(Co(CO)4) added to a cooled (-78°C) and stirred soln. of the Pd-complex, stirred for 0.25 h, dppm added, temp. raised to ambient, stirred for 8 h; filtered, n-hexane added, chromd. on silica gel impregnated with n-hexane, eluted with THF/n-hexane (1:1), recrystd. from THF/n-hexane, collected, elem. anal.;

Reference yield: 33.0%

: 14878-28-5
sodium tetracarbonyl cobaltate

: 38425-01-3
(bis(diphenylphosphino)methane)palladium(II) dichloride

: 2071-20-7
bis-diphenylphosphinomethane

: 113109-25-4
[Co2Pd(μ3-CO)(CO)4(μ-bis(diphenylphosphino)methane)2]

: 147958-30-3
ClPd((C₆H₅)2PCH₂P(C₆H₅)2)2Co(CO)2

Guidance literature:: In tetrahydrofuran; byproducts: CO, NaCl; soln. of the Co-complex added dropwise to a suspn. of the Pd-complex in THF at -30°C, dppm added after change of color at -20°C; chromd. using toluene;