5-(4-Carbamimidoyl-phenyl)-2-(naphthalene-1-sulfonylamino)-pentanoic acid phenylamide; hydriodide

Base Information

Chemical Name:5-(4-Carbamimidoyl-phenyl)-2-(naphthalene-1-sulfonylamino)-pentanoic acid phenylamide; hydriodide
CAS No.:83101-88-6
Molecular Formula:C₂₈H₂₈N₄O₃S*HI
Molecular Weight:628.534
Hs Code.:

Synonyms:

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Chemical Property of 5-(4-Carbamimidoyl-phenyl)-2-(naphthalene-1-sulfonylamino)-pentanoic acid phenylamide; hydriodide

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Technology Process of 5-(4-Carbamimidoyl-phenyl)-2-(naphthalene-1-sulfonylamino)-pentanoic acid phenylamide; hydriodide

There total 8 articles about 5-(4-Carbamimidoyl-phenyl)-2-(naphthalene-1-sulfonylamino)-pentanoic acid phenylamide; hydriodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.5%

: 83101-75-1
4-[4-(Naphthalene-1-sulfonylamino)-4-phenylcarbamoyl-butyl]-thiobenzimidic acid methyl ester; hydriodide

: 83101-88-6
5-(4-Carbamimidoyl-phenyl)-2-(naphthalene-1-sulfonylamino)-pentanoic acid phenylamide; hydriodide

Guidance literature:: With ammonium acetate; In ethanol; for 2.5h; Heating;

Reference yield:

: 35271-56-8,142917-82-6,1504-63-8
3-(4-nitrophenyl)propyl-2-en-1-ol

: 83101-88-6
5-(4-Carbamimidoyl-phenyl)-2-(naphthalene-1-sulfonylamino)-pentanoic acid phenylamide; hydriodide

Guidance literature:: Multi-step reaction with 8 steps

1: 78 percent / H₂ / Raney-Ni / methanol / 760 Torr

2: 1.) HCl/NaNO₂ / 1.) H₂O; 2.) 0-5 deg C 30 min, room temp. 4 h

3: PBr₃ / CHCl₃ / 1.5 h / Heating

4: C₂H₂ONa / ethanol / 5 h / Heating

6: 100 percent / TEA, H₂S / pyridine / Ambient temperature

7: 84 percent / acetone / Ambient temperature

8: 48.5 percent / 1.1M AcONH₄ / ethanol / 2.5 h / Heating

With hydrogenchloride; C₂H₂ONa; TEA; hydrogen sulfide; ammonium acetate; hydrogen; phosphorus tribromide; sodium nitrite; nickel; In pyridine; methanol; ethanol; chloroform; acetone;

Reference yield:

: 1734-79-8
3-(4-nitrophenyl)-2-propenal

: 83101-88-6
5-(4-Carbamimidoyl-phenyl)-2-(naphthalene-1-sulfonylamino)-pentanoic acid phenylamide; hydriodide

Guidance literature:: Multi-step reaction with 9 steps

1: 70 percent / NaBH₄ / methanol

2: 78 percent / H₂ / Raney-Ni / methanol / 760 Torr

3: 1.) HCl/NaNO₂ / 1.) H₂O; 2.) 0-5 deg C 30 min, room temp. 4 h

4: PBr₃ / CHCl₃ / 1.5 h / Heating

5: C₂H₂ONa / ethanol / 5 h / Heating

7: 100 percent / TEA, H₂S / pyridine / Ambient temperature

8: 84 percent / acetone / Ambient temperature

9: 48.5 percent / 1.1M AcONH₄ / ethanol / 2.5 h / Heating

With hydrogenchloride; sodium tetrahydroborate; C₂H₂ONa; TEA; hydrogen sulfide; ammonium acetate; hydrogen; phosphorus tribromide; sodium nitrite; nickel; In pyridine; methanol; ethanol; chloroform; acetone;