Technology Process of methyl boninenalate ethylene acetal
There total 10 articles about methyl boninenalate ethylene acetal which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) N-bromosuccinimide, 2.) K2CO3 / 1.) CCl4, reflux, 3 h, 2.) acetone, room temperature, 15 min; reflux, 2 h
2: 0.567 g / copper(II) sulphate / benzene / 10 h / Heating
With
N-Bromosuccinimide; potassium carbonate; copper(II) sulfate;
In
benzene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1.) N-bromosuccinimide, 2.) K2CO3 / 1.) CCl4, reflux, 3 h, 2.) acetone, room temperature, 15 min; reflux, 2 h
2: 0.567 g / copper(II) sulphate / benzene / 10 h / Heating
With
N-Bromosuccinimide; potassium carbonate; copper(II) sulfate;
In
benzene;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 5.047 g / conc.HCl / 9 h / Heating
2: 0.058 g / LiAlH4 / ethanol; diethyl ether / 0.5 h / Ambient temperature
3: 1.701 g / manganese dioxide / CCl4 / 1 h / Ambient temperature
4: 0.025 g / CF3COOH / 69 h / Ambient temperature
5: 1.) N-bromosuccinimide, 2.) K2CO3 / 1.) CCl4, reflux, 3 h, 2.) acetone, room temperature, 15 min; reflux, 2 h
6: 0.567 g / copper(II) sulphate / benzene / 10 h / Heating
With
hydrogenchloride; manganese(IV) oxide; N-Bromosuccinimide; lithium aluminium tetrahydride; potassium carbonate; copper(II) sulfate; trifluoroacetic acid;
In
tetrachloromethane; diethyl ether; ethanol; benzene;
