cis-bis(methylsulfanylacetato-O)bis(triphenylphosphine)platinum(II)

Base Information

Chemical Name:cis-bis(methylsulfanylacetato-O)bis(triphenylphosphine)platinum(II)
CAS No.:386704-80-9
Molecular Formula:C₄₂H₄₀O₄P₂PtS₂
Molecular Weight:929.937
Hs Code.:

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Chemical Property of cis-bis(methylsulfanylacetato-O)bis(triphenylphosphine)platinum(II)

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Technology Process of cis-bis(methylsulfanylacetato-O)bis(triphenylphosphine)platinum(II)

There total 3 articles about cis-bis(methylsulfanylacetato-O)bis(triphenylphosphine)platinum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 13517-35-6
tris(triphenylphosphine)platinum⁽⁰⁾

: 2444-37-3
methylsulfanyl-acetic acid

: 386704-80-9
cis-bis(methylsulfanylacetato-O)bis(triphenylphosphine)platinum(II)

Guidance literature:: In dichloromethane; byproducts: H2; soln. methylsulfanylacetic acid in CH2Cl2 was added to cold (ice bath) soln. (Pt(PPh3)3) in CH2Cl2 under N2 atm.; soln. was kept for 2 h in the cold and concd. in vacuo, diisopropyl ether was added;
DOI:10.1016/j.ica.2004.09.039

Reference yield: 88.0%

: 348615-93-0
[Pt(PPh₃)2((methylsulfanyl)acetate-O,S)]NO₃

: (methylsulfanyl)acetic acid potassium salt

: 386704-80-9
cis-bis(methylsulfanylacetato-O)bis(triphenylphosphine)platinum(II)

Guidance literature:: In dichloromethane; to potassium methylsulfanylacetate (Pt(PPh3)2(methylsulfanylacetate-O,S))NO3 was added and refluxed for 8 h; soln. was filtered and concd. in vacuo, diisopropyl ether was added; elem. anal.;
DOI:10.1016/j.ica.2004.09.039

Reference yield:

: 1140481-03-3,16009-24-8,17611-57-3
cis-[bis(triphenylphosphane)bis(nitrato)platinul(II)]

: (methylsulfanyl)acetic acid potassium salt

: 386704-80-9
cis-bis(methylsulfanylacetato-O)bis(triphenylphosphine)platinum(II)

Guidance literature:: In dichloromethane; potassium methylsulfanylacetate and cis-(Pt(PPh3)2(NO3)2) in CH2Cl2 wererefluxed for 8 h; soln. was concd., diisopropyl ether was added;
DOI:10.1016/j.ica.2004.09.039