bis(benzylmethyl ketone thiosemicarbazonato)nickel(II)

Base Information

• Chemical Name: bis(benzylmethyl ketone thiosemicarbazonato)nickel(II)
• CAS No.: 86742-57-6
• Molecular Formula: C₂₀H₂₄N₆NiS₂
• Molecular Weight: 471.273
• Mol file: 86742-57-6.mol

Synonyms:

Chemical Property of bis(benzylmethyl ketone thiosemicarbazonato)nickel(II)

Chemical Property:

Purity/Quality:

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MSDS Files:

Useful:

Technology Process of bis(benzylmethyl ketone thiosemicarbazonato)nickel(II)

There total 1 articles about bis(benzylmethyl ketone thiosemicarbazonato)nickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

benzyl methyl ketone thiosemicarbazone (19091-42-0) + nickel dichloride (83864-14-6) → bis(benzylmethyl ketone thiosemicarbazonato)nickel(II) (86742-57-6)

Guidance literature:

In ethanol; ammonia; aq. ammonia=NH3; to ammonia soln. of metal chloride hot 95% EtOH soln. of thiosemicarbazone is added, mixt. refluxed for 1 h; cooled, filtered, washed with water, EtOH, dried at 60°C; elem. anal.;

upstream raw materials:

benzyl methyl ketone thiosemicarbazone

nickel dichloride