1,2-bis[(2,6-diisopropylphenyl)imino]acenaphthene-molybdenumtetracarbonyl

Base Information

• Chemical Name: 1,2-bis[(2,6-diisopropylphenyl)imino]acenaphthene-molybdenumtetracarbonyl
• CAS No.: 1176801-01-6
• Molecular Formula: C₄₀H₄₀MoN₂O₄
• Molecular Weight: 708.709
• Mol file: 1176801-01-6.mol

Synonyms:

Chemical Property of 1,2-bis[(2,6-diisopropylphenyl)imino]acenaphthene-molybdenumtetracarbonyl

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of 1,2-bis[(2,6-diisopropylphenyl)imino]acenaphthene-molybdenumtetracarbonyl

There total 1 articles about 1,2-bis[(2,6-diisopropylphenyl)imino]acenaphthene-molybdenumtetracarbonyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

molybdenum hexacarbonyl (13939-06-5,199620-15-0) + 1,2-bis-[(2,6-diisopropylphenyl)imino]acenaphthene (153625-67-3) → 1,2-bis[(2,6-diisopropylphenyl)imino]acenaphthene-molybdenumtetracarbonyl (1176801-01-6)

Guidance literature:

In toluene; byproducts: CO; (Schlenk) to a soln. of acenaphthene-compound in toluene Mo(CO)6 was added, reflux for 12 h; the solvent was evapd. under vac., crystd. from hexane; elem. anal.;

DOI:10.1039/b902709b

upstream raw materials:

molybdenum hexacarbonyl

1,2-bis-[(2,6-diisopropylphenyl)imino]acenaphthene