oxo(5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)chromium(IV)

Base Information

Chemical Name:oxo(5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)chromium(IV)
CAS No.:94890-09-2
Molecular Formula:C₄₄H₈CrF₂₀N₄O
Molecular Weight:1040.54
Hs Code.:

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Chemical Property of oxo(5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)chromium(IV)

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Technology Process of oxo(5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)chromium(IV)

There total 2 articles about oxo(5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)chromium(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 94890-04-7
chloro(5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)chromium(III)

: 536-80-1
iodosylbenzene

: 94890-09-2
oxo(5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)chromium(IV)

Guidance literature:: In dichloromethane; under N2; deoxygenated CH2Cl2 was transferred to a mixt. of 1 equiv of Cr-complex and 12 equiv of iodosylbenzene; mixt. stirred for 20 min; chromy. on basic alumina column, eluted with CH2Cl2; evapn. under reduced pressure, dry heptane slowly added, filtered, washed with heptane; elem. anal.;

Reference yield:

: 94890-04-7
chloro(5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)chromium(III)

: 94890-09-2
oxo(5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)chromium(IV)

Guidance literature:: With zinc amalgam; O₂; In tetrahydrofuran; the Cr-complex was reduced in THF with amalgamated Zn under N2; evapn. to dryness under reduced pressure, extn. with degassed toluene; dry O2 was bubbled through the soln.; not isolated;