[Mo(η3-methallyl)(tert-butyl isocyanide)(4,4'-bis((4-methylphenyl)carbamoyl)-2,2'-bipyridine)(CO)2][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]

Base Information

Chemical Name:[Mo(η3-methallyl)(tert-butyl isocyanide)(4,4'-bis((4-methylphenyl)carbamoyl)-2,2'-bipyridine)(CO)2][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]
CAS No.:934187-30-1
Molecular Formula:C₃₂H₁₂BF₂₄*C₃₇H₃₈MoN₅O₄
Molecular Weight:1575.9
Hs Code.:

[Mo(η3-methallyl)(tert-butyl isocyanide)(4,4'-bis((4-methylphenyl)carbamoyl)-2,2'-bipyridine)(CO)2][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]

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Chemical Property of [Mo(η3-methallyl)(tert-butyl isocyanide)(4,4'-bis((4-methylphenyl)carbamoyl)-2,2'-bipyridine)(CO)2][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]

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Technology Process of [Mo(η3-methallyl)(tert-butyl isocyanide)(4,4'-bis((4-methylphenyl)carbamoyl)-2,2'-bipyridine)(CO)2][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]

There total 1 articles about [Mo(η3-methallyl)(tert-butyl isocyanide)(4,4'-bis((4-methylphenyl)carbamoyl)-2,2'-bipyridine)(CO)2][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: [Mo(η3-methallyl)Cl(CO)2(acetonitrile)2]

: 934187-26-5
4,4'-bis((4-methylphenyl)carbamoyl)-2,2'-bipyridine

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 79060-88-1
sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

: 934187-30-1
[Mo(η3-methallyl)(tert-butyl isocyanide)(4,4'-bis((4-methylphenyl)carbamoyl)-2,2'-bipyridine)(CO)2][tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]

Guidance literature:: In dichloromethane; acetonitrile; byproducts: NaCl; (N2); Na salt and MeCN added to a soln. of Mo complex in CH2Cl2, stirredat room temp. for 5 min, filtered, evapd., dissolved in THF, (C5H3NC(O) NHC6H4CH3)2 added, stirred at room temp. for 20 min, CNC(CH3)3 added, stirred for 30 min; concd. (vac.), pptd. (hexane), washed (hexane); elem. anal.;
DOI:10.1021/ic0621650