Technology Process of Perrottetin G triacetat
There total 9 articles about Perrottetin G triacetat which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
pyridine;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 37 percent / K2CO3; CuO / pyridine / 48 h / 120 °C
2: 76 percent / K2CO3 / acetone / 5 h / Heating
3: 91 percent / LiAlH4 / tetrahydrofuran
4: 80 percent / PBr3 / CH2Cl2 / 3 h / Ambient temperature
5: 93 percent / acetonitrile / 1 h / Heating
6: 1N NaOCH3, / CH2Cl2 / 1 h
7: 77 percent / H2 / Pd/C / acetic acid
8: 88 percent / pyridine / Ambient temperature
With
lithium aluminium tetrahydride; hydrogen; sodium methylate; phosphorus tribromide; potassium carbonate; copper(II) oxide;
palladium on activated charcoal;
In
tetrahydrofuran; pyridine; dichloromethane; acetic acid; acetone; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 37 percent / K2CO3; CuO / pyridine / 48 h / 120 °C
2: 76 percent / K2CO3 / acetone / 5 h / Heating
3: 91 percent / LiAlH4 / tetrahydrofuran
4: 80 percent / PBr3 / CH2Cl2 / 3 h / Ambient temperature
5: 93 percent / acetonitrile / 1 h / Heating
6: 1N NaOCH3, / CH2Cl2 / 1 h
7: 77 percent / H2 / Pd/C / acetic acid
8: 88 percent / pyridine / Ambient temperature
With
lithium aluminium tetrahydride; hydrogen; sodium methylate; phosphorus tribromide; potassium carbonate; copper(II) oxide;
palladium on activated charcoal;
In
tetrahydrofuran; pyridine; dichloromethane; acetic acid; acetone; acetonitrile;