Technology Process of Phenol,5-[2-(3-hydroxyphenyl)ethyl]-3-[4-[2-(3-hydroxyphenyl)ethyl]phenoxy]-2-methoxy-
There total 13 articles about Phenol,5-[2-(3-hydroxyphenyl)ethyl]-3-[4-[2-(3-hydroxyphenyl)ethyl]phenoxy]-2-methoxy- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
methanol;
at 20 ℃;
for 12h;
under 3750.3 Torr;
DOI:10.1055/s-1991-26496
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 80 percent / PBr3 / CH2Cl2 / 3 h / Ambient temperature
2: 93 percent / acetonitrile / 1 h / Heating
3: 1N NaOCH3, / CH2Cl2 / 1 h
4: 77 percent / H2 / Pd/C / acetic acid
With
hydrogen; sodium methylate; phosphorus tribromide;
palladium on activated charcoal;
In
dichloromethane; acetic acid; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1N NaOCH3, / CH2Cl2 / 1 h
2: 77 percent / H2 / Pd/C / acetic acid
With
hydrogen; sodium methylate;
palladium on activated charcoal;
In
dichloromethane; acetic acid;
