(μ-(phenyl)CN(phenyl))(μ-methylthiolate)diiron hexacarbonyl

Base Information

Chemical Name:(μ-(phenyl)CN(phenyl))(μ-methylthiolate)diiron hexacarbonyl
CAS No.:111905-37-4
Molecular Formula:C₂₀H₁₃Fe₂NO₆S
Molecular Weight:507.086
Hs Code.:

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Chemical Property of (μ-(phenyl)CN(phenyl))(μ-methylthiolate)diiron hexacarbonyl

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Technology Process of (μ-(phenyl)CN(phenyl))(μ-methylthiolate)diiron hexacarbonyl

There total 3 articles about (μ-(phenyl)CN(phenyl))(μ-methylthiolate)diiron hexacarbonyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: lithium{(μ-carbonyl)(μ-methylthiolate)diiron hexacarbonyl}

: 4903-36-0
N-phenyl-benzimidoyl chloride

: 111905-37-4
(μ-(phenyl)CN(phenyl))(μ-methylthiolate)diiron hexacarbonyl

: bis(methylthio)hexacarbonyldiiron

Guidance literature:: In tetrahydrofuran; Under N2, addn. of PhC(Cl)NPh to soln. of Li-Fe-complex, stirring (60 h, room temp.).; Evapn. of solvent in vac. yields a brown-red tar, filtn. chromy. (silicic acid, pentane) gives orange band of (MeS)2Fe-complex ((1)H NMR), further elution yields a second orange band.;

Reference yield: 43.0%

: 17685-52-8
triiron dodecarbonyl

: 6780-43-4,52019-85-9
S-methyl N-phenylbenzenecarboximidothioate

: 111905-37-4
(μ-(phenyl)CN(phenyl))(μ-methylthiolate)diiron hexacarbonyl

: bis(methylthio)hexacarbonyldiiron

Guidance literature:: In hexane; Degassing of mixt. with N2, addn. of hexane, resulting dark green soln. is refluxed for 28 h, soln. turns red.; Evapn. in vac., red oily residue is purified by filtration chromy. (silicic acid, pentane) gives first S2-complex ((1)H NMR), further elution of an orange band, recrystn. (pentane), elem. anal.;

Reference yield:

: 15321-51-4
diiron nonacarbonyl

: 6780-43-4,52019-85-9
S-methyl N-phenylbenzenecarboximidothioate

: 111905-37-4
(μ-(phenyl)CN(phenyl))(μ-methylthiolate)diiron hexacarbonyl

: bis(methylthio)hexacarbonyldiiron

Guidance literature:: In hexane; Degassing of mixt. with N2, addn. of hexane, resulting dark green soln. is refluxed for 28 h, soln. turns red.; Evapn. in vac., red oily residue is purified by filtration chromy. (silicic acid, pentane) gives first S2-complex ((1)H NMR), further elution of an orange band, recrystn. (pentane).;