4-nitro-O-acetylbenzoin

Base Information

• Chemical Name: 4-nitro-O-acetylbenzoin
• CAS No.: 135490-87-8
• Molecular Formula: C₁₆H₁₃NO₅
• Molecular Weight: 299.283

Synonyms:

Chemical Property of 4-nitro-O-acetylbenzoin

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

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Technology Process of 4-nitro-O-acetylbenzoin

There total 1 articles about 4-nitro-O-acetylbenzoin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

acetic anhydride (108-24-7) + 2-hydroxy-2-phenylacetophenone (119-53-9,579-44-2) → 4-nitro-O-acetylbenzoin (135490-87-8)

Guidance literature:

With sulfuric acid; potassium nitrate; at -5 ℃; for 72h;

Reference yield: 54.0%

4-nitro-O-acetylbenzoin (135490-87-8) → 4-nitrobenzil (22711-24-6)

Guidance literature:

With nitric acid; at 90 ℃;

upstream raw materials:

acetic anhydride

2-hydroxy-2-phenylacetophenone

Downstream raw materials:

4-nitrobenzil

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