1-(4-Nitrophenyl)-2-phenylethane-1,2-dione

Base Information

Chemical Name:1-(4-Nitrophenyl)-2-phenylethane-1,2-dione
CAS No.:22711-24-6
Molecular Formula:C14H9 N O4
Molecular Weight:255.23
Hs Code.:2914700090
NSC Number:139153
DSSTox Substance ID:DTXSID10300826
Nikkaji Number:J359.703B
Wikidata:Q82044199
Pharos Ligand ID:F7KZTG6FSGU4
ChEMBL ID:CHEMBL192589
Mol file:22711-24-6.mol

Synonyms:1-(4-nitrophenyl)-2-phenylethane-1,2-dione;22711-24-6;4-Nitrobenzil;1,2-Ethanedione,1-(4-nitrophenyl)-2-phenyl-;p-Nitrobenzil;Benzil, 4-nitro-;Ethanedione, (4-nitrophenyl)phenyl-;NSC139153;Benzil-based compound, 27;1-(4-Nitro-phenyl)-2-phenyl-ethane-1,2-dione;CHEMBL192589;SCHEMBL1370034;BDBM22749;DTXSID10300826;GPDKREBNFFEDHW-UHFFFAOYSA-N;STK325617;AKOS004902243;NSC-139153;PD129620;4-(Bromonethyl)-N-(l-methylethy)benzamide;FT-0605764

Suppliers and Price of 1-(4-Nitrophenyl)-2-phenylethane-1,2-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-(4-NITROPHENYL)-2-PHENYLETHANE-1,2-DIONE 95.00%
1G
$ 713.10

AHH
1-(4-Nitrophenyl)-2-phenylethane-1,2-dione 95%
10g
$ 346.00

Total 13 raw suppliers

Chemical Property of 1-(4-Nitrophenyl)-2-phenylethane-1,2-dione

Chemical Property:

Vapor Pressure:4.14E-08mmHg at 25°C
Melting Point:141oC
Boiling Point:444.9°Cat760mmHg
Flash Point:220.9°C
PSA：79.96000
Density:1.327g/cm³
LogP:3.18360
XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:255.05315777
Heavy Atom Count:19
Complexity:360

Purity/Quality:

98%min ^*data from raw suppliers

1-(4-NITROPHENYL)-2-PHENYLETHANE-1,2-DIONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes: Xi:Irritant;
Statements: R36/37/38:Irritating to eyes, respiratory system and skin.;
Safety Statements: S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.; S37/39:Wear suitable g

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=O)C(=O)C2=CC=C(C=C2)[N+](=O)[O-]

Technology Process of 1-(4-Nitrophenyl)-2-phenylethane-1,2-dione

There total 55 articles about 1-(4-Nitrophenyl)-2-phenylethane-1,2-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1942-30-9
4-(phenylethynyl)nitrobenzene

: 22711-24-6
4-nitrobenzil

Guidance literature:: With 2-chloropyridine-N-oxide; iodine; In acetonitrile; at 80 ℃; for 12h; Reagent/catalyst; Temperature; chemoselective reaction; Sealed tube;
DOI:10.1021/acs.joc.8b00484

Reference yield: 100.0%

: 2-(4-Nitro-phenyl)-1-phenyl-2-[(Z)-phenylimino]-ethanone

: 22711-24-6
4-nitrobenzil

Guidance literature:: With hydrogenchloride; water; In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1016/j.tet.2011.04.020

Reference yield: 91.0%

: 17763-80-3
para-nitrophenyl triflate

: 536-74-3
phenylacetylene

: 22711-24-6
4-nitrobenzil

Guidance literature:: para-nitrophenyl triflate; phenylacetylene; With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In dimethyl sulfoxide; at 90 ℃; for 4h; Schlenk technique; Inert atmosphere;

With oxygen; at 150 ℃; for 20h;
DOI:10.1002/ejoc.201900783