(C₅H₅(CO)Fe(C(CN)CH₂))2(C₆H₅)2PCH₂CH₂P(C₆H₅)2

Base Information

Chemical Name:(C₅H₅(CO)Fe(C(CN)CH₂))2(C₆H₅)2PCH₂CH₂P(C₆H₅)2
CAS No.:114657-26-0
Molecular Formula:C₄₄H₃₈Fe₂N₂O₂P₂
Molecular Weight:800.439
Hs Code.:

(C<sub>5</sub>H<sub>5</sub>(CO)Fe(C(CN)CH<sub>2</sub>))2(C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2

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Chemical Property of (C₅H₅(CO)Fe(C(CN)CH₂))2(C₆H₅)2PCH₂CH₂P(C₆H₅)2

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Technology Process of (C₅H₅(CO)Fe(C(CN)CH₂))2(C₆H₅)2PCH₂CH₂P(C₆H₅)2

There total 1 articles about (C₅H₅(CO)Fe(C(CN)CH₂))2(C₆H₅)2PCH₂CH₂P(C₆H₅)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 74915-04-1
C₅H₅FeCOHP(C₆H₅)2CH₂CH₂P(C₆H₅)2FeCOHC₅H₅

: 1070-71-9
propiolonitrile

: 114657-26-0
(C₅H₅(CO)Fe(C(CN)CH₂))2(C₆H₅)2PCH₂CH₂P(C₆H₅)2

Guidance literature:: In toluene; the iron-complex in toluene is frozen in liquid nitrogen and the cyano-compd. is condensed into the reaction tube, the mixt. is stirred at roomtemp. for 6-40 h (using Schlenk technique); the soln. is concd. and filtered through a Celite pad, detection of mixt. of isomers by (31)P-NMR, addition of hexane, crystn. of first isomer,chromy. of the supernatant liquid, elution of second isomer with CH2Cl2/THF, elem. anal.;
DOI:10.1016/S0022-328X(00)99754-7