1-Propanamine,3,3'-thiobis-

Base Information

• Chemical Name: 1-Propanamine,3,3'-thiobis-
• CAS No.: 13643-20-4
• Molecular Formula: C6H16 N2 S
• Molecular Weight: 148.272
• Mol file: 13643-20-4.mol

Synonyms:Propylamine,3,3'-thiobis- (7CI,8CI); 1,9-Diaza-5-thianonane; 3,3'-Thiobispropylamine;3,3'-Thiodipropylamine; 4-Thia-1,7-heptanediamine; Bis(3-aminopropyl) sulfide;Homolanthionamine

Chemical Property of 1-Propanamine,3,3'-thiobis-

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Propanamine,3,3'-thiobis-

There total 1 articles about 1-Propanamine,3,3'-thiobis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-amino-2-propene (107-11-9,30551-89-4) → mercapto-3 propylamine (462-47-5) + 3,3'-diamino propyl thioether (13643-20-4)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); hydrogen sulfide; at 90 ℃;

Reference yield:

3,3'-diamino propyl thioether (13643-20-4) + C21H15BrF3N3O3 (1149764-38-4) + 3(3-Aminopropylthio)propionitril (16496-87-0) → C26H22F3N5O2S (1150268-05-5) + C46H36F6N8O4S (1150268-08-8)

Guidance literature:

With sodium hydrogencarbonate; In acetonitrile; for 2h; Heating / reflux;

Reference yield:

3,3'-diamino propyl thioether (13643-20-4) + 2-Nitrobenzenesulfonyl chloride (1694-92-4) → N,N'-bis(2-nitrobenzenesulfonyl)-bis(3-aminopropyl) thioether (344950-71-6)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; Inert atmosphere;

DOI:10.1021/jm901530b

upstream raw materials:

1-amino-2-propene

Downstream raw materials:

C₂₆H₂₂F₃N₅O₂S

C₄₆H₃₆F₆N₈O₄S

N,N'-bis(2-nitrobenzenesulfonyl)-bis(3-aminopropyl) thioether

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